2,6-Diacetamidobenzoic acid

Base Information

• Chemical Name: 2,6-Diacetamidobenzoic acid
• CAS No.: 7758-61-4
• Molecular Formula: C₁₁H₁₂N₂O₄
• Molecular Weight: 236.227
• Mol file: 7758-61-4.mol

Synonyms:Benzoic acid,2,6-diacetamido;2,6-Bis-acetamino-benzoesaeure;2,6-Diacetylaminobenzoesaeure;

Chemical Property of 2,6-Diacetamidobenzoic acid

Chemical Property:

• Vapor Pressure: 1.03E-12mmHg at 25°C
• Boiling Point: 545.1°Cat760mmHg
• Flash Point: 283.5°C
• PSA: 102.48000
• Density: 1.404g/cm³
• LogP: 2.60060

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-Diacetamidobenzoic acid

There total 1 articles about 2,6-Diacetamidobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2,6-di(acetylamino)benzoic acid (7758-61-4)

Guidance literature:

2,6-Diacetylaminotoluid (8b), Bamberger Oxyd.;

Reference yield: 60.6%

copper(ll) sulfate pentahydrate + 2,6-di(acetylamino)benzoic acid (7758-61-4) + water (7732-18-5) → [Cu(II)(2,6-di(acetylamino)benzoate)(H2O)2] * H2O

Guidance literature:

With KHCO₃; In water; slow addn. of CuSO4 to mixt. of 2 equiv. ligand and 2 equiv. KHCO3; crystn. (12 h); elem. anal.;

DOI:10.1016/s0020-1693(97)06144-6

Reference yield: 23.4%

2,6-di(acetylamino)benzoic acid (7758-61-4) + water (7732-18-5) + magnesium(II) acetate tetrahydrate (16674-78-5) → C22H30MgN4O12

Guidance literature:

2,6-di(acetylamino)benzoic acid; magnesium(II) acetate tetrahydrate; In methanol; Heating;

water; In methanol; at 20 ℃; for 168h;

DOI:10.1021/ic400671v

Downstream raw materials:

2,6-diaminobenzoic acid

Refernces