2-(((2-Amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-9,10-anthracenedione

Base Information

Chemical Name:2-(((2-Amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-9,10-anthracenedione
CAS No.:102830-99-9
Molecular Formula:C₂₁H₂₁NO₈
Molecular Weight:415.4
Hs Code.:
DSSTox Substance ID:DTXSID30908080
Wikidata:Q82877464

Synonyms:102830-99-9;2-(((2-Amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-9,10-anthracenedione;DTXSID30908080;9,10-Anthracenedione, 2-(((2-amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-;(1-Hydroxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl 2-amino-2-deoxyhexopyranoside

Suppliers and Price of 2-(((2-Amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-9,10-anthracenedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(((2-Amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-9,10-anthracenedione

Chemical Property:

Vapor Pressure:3.07E-21mmHg at 25°C
Boiling Point:711.4°Cat760mmHg
Flash Point:384°C
Density:1.59g/cm³
XLogP3:0.3
Hydrogen Bond Donor Count:5
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:4
Exact Mass:415.12671663
Heavy Atom Count:30
Complexity:659

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=O)C3=C(C2=O)C(=C(C=C3)COC4C(C(C(C(O4)CO)O)O)N)O
Isomeric SMILES:C1=CC=C2C(=C1)C(=O)C3=C(C2=O)C(=C(C=C3)CO[C@H]4[C@@H]([C@H]([C@@H]([C@H](O4)CO)O)O)N)O

Technology Process of 2-(((2-Amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-9,10-anthracenedione

There total 3 articles about 2-(((2-Amino-2-deoxy-beta-D-glucopyranosyl)oxy)methyl)-1-hydroxy-9,10-anthracenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 102830-94-4
1-hydroxy-2-<<3,4,6-tri-O-acetyl-2-deoxy-2-<(trifluoroacetyl)amino>-β-D-glucosyloxy>methyl>-9,10-dihydro-9,10-anthracenedione

: 102830-99-9
1-hydroxy-2-<(2-deoxy-2-amino-β-D-glucosyloxy)methyl>-9,10-dihydro-9,10-anthracenedione

Guidance literature:: With sodium hydroxide; In acetone; for 4h; Ambient temperature;
DOI:10.1021/jm00159a024

Reference yield:

: 6736-63-6
3,4,6-tri-O-acetyl-2-deoxy-2-trifluoroacetamido-α-D-glucospyranosyl bromide

: 102830-99-9
1-hydroxy-2-<(2-deoxy-2-amino-β-D-glucosyloxy)methyl>-9,10-dihydro-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / silver trifluoromethanesulfonate, molecular sieve 3A / CH₂Cl₂ / 4 h / Ambient temperature

2: 47 percent / 0.1 N NaOH / acetone / 4 h / Ambient temperature

With sodium hydroxide; 3 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; acetone;
DOI:10.1021/jm00159a024

Reference yield:

: 24094-45-9
digiferruginol

: 102830-99-9
1-hydroxy-2-<(2-deoxy-2-amino-β-D-glucosyloxy)methyl>-9,10-dihydro-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / silver trifluoromethanesulfonate, molecular sieve 3A / CH₂Cl₂ / 4 h / Ambient temperature

2: 47 percent / 0.1 N NaOH / acetone / 4 h / Ambient temperature

With sodium hydroxide; 3 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; acetone;
DOI:10.1021/jm00159a024