5H-Imidazo(2,1-c)(1,4)benzodiazepine, 7,8-dimethoxy-

Base Information

Chemical Name:5H-Imidazo(2,1-c)(1,4)benzodiazepine, 7,8-dimethoxy-
CAS No.:98234-92-5
Molecular Formula:C₁₃H₁₃N₃O₂
Molecular Weight:243.265
Hs Code.:
DSSTox Substance ID:DTXSID80243519

Synonyms:7,8-Dimethoxy-5H-imidazo(2,1-c)(1,4)benzodiazepine;5H-Imidazo(2,1-c)(1,4)benzodiazepine, 7,8-dimethoxy-;98234-92-5;DTXSID80243519;LS-77790

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5H-Imidazo(2,1-c)(1,4)benzodiazepine, 7,8-dimethoxy-

Chemical Property:

Vapor Pressure:8.38E-10mmHg at 25°C
Boiling Point:491.4°Cat760mmHg
Flash Point:251°C
Density:1.29g/cm³
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:243.100776666
Heavy Atom Count:18
Complexity:323

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C2C(=C1)CN3C=CN=C3C=N2)OC

Technology Process of 5H-Imidazo(2,1-c)(1,4)benzodiazepine, 7,8-dimethoxy-

There total 4 articles about 5H-Imidazo(2,1-c)(1,4)benzodiazepine, 7,8-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.3%

: 98235-06-4
1-(4,5-Dimethoxy-2-nitro-benzyl)-1H-imidazole-2-carbaldehyde

: 98234-92-5
6,7-Dimethoxy-4H-1,3a,9-triaza-benzo[f]azulene

Guidance literature:: With ammonium hydroxide; iron(II) sulfate; In ethanol; water; at 120 ℃; for 1h;

Reference yield:

: 15862-94-9
1-(chloromethyl)-4,5-dimethoxy-2-nitrobenzene

: 98234-92-5
6,7-Dimethoxy-4H-1,3a,9-triaza-benzo[f]azulene

Guidance literature:: Multi-step reaction with 4 steps

1: 53.2 percent / Na₂CO₃ / dimethylformamide / 3 h / 125 °C

2: 50.4 percent / H₂O / 115 °C / sealed tube, overnight

3: 90.6 percent / activated MnO₂ / acetone / Ambient temperature

4: 86.3 percent / iron(II) sulphate heptahydrate, NH₄OH 32percent / ethanol; H₂O / 1 h / 120 °C

With manganese(IV) oxide; ammonium hydroxide; sodium carbonate; iron(II) sulfate; In ethanol; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 98234-98-1
1-(4,5-Dimethoxy-2-nitro-benzyl)-1H-imidazole

: 98234-92-5
6,7-Dimethoxy-4H-1,3a,9-triaza-benzo[f]azulene

Guidance literature:: Multi-step reaction with 3 steps

1: 50.4 percent / H₂O / 115 °C / sealed tube, overnight

2: 90.6 percent / activated MnO₂ / acetone / Ambient temperature

3: 86.3 percent / iron(II) sulphate heptahydrate, NH₄OH 32percent / ethanol; H₂O / 1 h / 120 °C

With manganese(IV) oxide; ammonium hydroxide; iron(II) sulfate; In ethanol; water; acetone;