1,10-Phenanthroline, 3,8-diphenyl-

Base Information

Chemical Name:1,10-Phenanthroline, 3,8-diphenyl-
CAS No.:95942-95-3
Molecular Formula:C24H16N2
Molecular Weight:332.404
Hs Code.:
Mol file:95942-95-3.mol

Synonyms:3,8-diphenyl-[1,10]phenanthroline;3,8-diphenyl-1,10-phenanthroline;3,8-Diphenyl-[1,10]phenanthrolin;3,8 -diphenyl-1,10-phenanthroline;

Suppliers and Price of 1,10-Phenanthroline, 3,8-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,10-Phenanthroline, 3,8-diphenyl-

Chemical Property:

Melting Point:189 - 191 °C
Boiling Point:549.2±45.0 °C(Predicted)
PSA：25.78000
Density:1.210±0.06 g/cm3(Predicted)
LogP:6.11700

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,10-Phenanthroline, 3,8-diphenyl-

There total 9 articles about 1,10-Phenanthroline, 3,8-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1422669-86-0
2,9-dichloro-3,8-diphenyl-1,10-phenanthroline

: 95942-95-3
3,8-bis(phenyl)-1,10-phenanthroline

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c2ob27325j

Reference yield: 81.0%

: 100125-12-0
3,8-dibromo-1,10-phenathroline

: 98-80-6
phenylboronic acid

: 95942-95-3
3,8-bis(phenyl)-1,10-phenanthroline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; toluene; for 18h; Inert atmosphere; Reflux;
DOI:10.1021/ja201873d

Reference yield:

: 66-71-7
1,10-Phenanthroline

: 95942-95-3
3,8-bis(phenyl)-1,10-phenanthroline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; disulfur dichloride; bromine / n-Butyl chloride / 12 h / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 24 h / 115 °C / Inert atmosphere

With pyridine; disulfur dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; sodium carbonate; In ethanol; n-Butyl chloride; water; toluene; 2: Suzuki coupling;
DOI:10.1016/j.jphotochem.2012.05.017