2,4,5-Tribromoanisole

Base Information

Chemical Name:2,4,5-Tribromoanisole
CAS No.:95970-10-8
Molecular Formula:C7H5Br3O
Molecular Weight:344.828
Hs Code.:
NSC Number:134564
DSSTox Substance ID:DTXSID401304439
Nikkaji Number:J1.617.523D
Mol file:95970-10-8.mol

Synonyms:2,4,5-Tribromoanisole;95970-10-8;1,2,4-tribromo-5-methoxybenzene;NSC134564;DTXSID401304439;NSC-134564

Suppliers and Price of 2,4,5-Tribromoanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2,4,5-Tribromoanisole
1g
$ 1490.00

Alichem
2,4,5-Tribromoanisole
500mg
$ 823.15

Alichem
2,4,5-Tribromoanisole
250mg
$ 480.00

Total 0 raw suppliers

Chemical Property of 2,4,5-Tribromoanisole

Chemical Property:

Melting Point:105°C
Refractive Index:1.5580 (estimate)
Boiling Point:307°C (rough estimate)
PSA：9.23000
Density:2.2119 (rough estimate)
LogP:3.98270
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:343.78700
Heavy Atom Count:11
Complexity:131

Purity/Quality:: 2,4,5-Tribromoanisole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1Br)Br)Br

Technology Process of 2,4,5-Tribromoanisole

There total 18 articles about 2,4,5-Tribromoanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 488-48-2
tetrabromobenzoquinone

: 95970-10-8
2,4,5-tribromo-anisole

Guidance literature:: With potassium nitrate; potassium bromide; In water; trifluoroacetic acid; at 20 ℃; for 8h; Product distribution;

Reference yield: 1.12%

: 2398-37-0
3-methoxyphenyl bromide

: 95970-10-8
2,4,5-tribromo-anisole

: 62415-74-1
3,4-dibromoanisole

: 95970-22-2
1,2-dibromo-3-methoxybenzene

Guidance literature:: With (CH₃)4Br; In liquid sulphur dioxide; at -23 ℃; Rate constant; Product distribution;
DOI:10.1002/hlca.19830660410

Reference yield:

: 93-26-5
2-methoxyacetanilide

: 95970-10-8
2,4,5-tribromo-anisole

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Br₂ / acetic acid

2: 73.6 percent / conc. HCl / ethanol / 3 h / Heating

3: 1.) aq. H₂SO₄, NaNO₂, 2.) Cu₂Br₂, conc. HBr; / 1.) acetic acid, 0 deg C, 30 min, 2.) 0 deg C, 30 min, 3.) from 0 deg C, to 100 deg C, 1.5 h;

With copper(I) bromide; hydrogenchloride; sulfuric acid; hydrogen bromide; bromine; sodium nitrite; In ethanol; acetic acid;