2-Propen-1-one, 1-(3,5-dichlorophenyl)-3-(dimethylamino)-

Base Information

Chemical Name:2-Propen-1-one, 1-(3,5-dichlorophenyl)-3-(dimethylamino)-
CAS No.:96604-27-2
Molecular Formula:C11H11Cl2NO
Molecular Weight:244.12
Hs Code.:
DSSTox Substance ID:DTXSID60426888

Synonyms:2-Propen-1-one, 1-(3,5-dichlorophenyl)-3-(dimethylamino)-;DTXSID60426888;BKUHHZMAJCOLAZ-UHFFFAOYSA-N;1-(3,5-dichlorophenyl)-3-dimethylamino-2-propen-1-one

Suppliers and Price of 2-Propen-1-one, 1-(3,5-dichlorophenyl)-3-(dimethylamino)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-(3,5-Dichlorophenyl)-N,N-dimethylacrylamide 97%
1g
$ 583.00

Total 0 raw suppliers

Chemical Property of 2-Propen-1-one, 1-(3,5-dichlorophenyl)-3-(dimethylamino)-

Chemical Property:

PSA：20.31000
LogP:3.25140
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:243.0217694
Heavy Atom Count:15
Complexity:243

Purity/Quality:: 3-(3,5-Dichlorophenyl)-N,N-dimethylacrylamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C=CC(=O)C1=CC(=CC(=C1)Cl)Cl

Technology Process of 2-Propen-1-one, 1-(3,5-dichlorophenyl)-3-(dimethylamino)-

There total 1 articles about 2-Propen-1-one, 1-(3,5-dichlorophenyl)-3-(dimethylamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14401-72-0
3',5'-dichloroacetophenone

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 96604-27-2
1-(3,5-dichlorophenyl)-3-(dimethylamino)-2-propen-1-one

Guidance literature:: at 90 ℃; for 2h;
DOI:10.1016/S0040-4020(02)01487-4

Reference yield:

: 96604-27-2
1-(3,5-dichlorophenyl)-3-(dimethylamino)-2-propen-1-one

: 154257-66-6
3-(3,5-dichlorophenyl)-1H-pyrazole

Guidance literature:: With hydrazine hydrate; In ethanol; at 20 ℃; for 2h;
DOI:10.1016/S0040-4020(02)01487-4

Reference yield:

: 96604-27-2
1-(3,5-dichlorophenyl)-3-(dimethylamino)-2-propen-1-one

: [3-(3,5-dichlorophenyl)-1-ethyl-1H-pyrazol-4-yl]phenylmethanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrazine hydrate / ethanol; water / 18 h / 20 °C

2.1: N-iodo-succinimide / acetonitrile / 24 h / 20 °C

3.1: isopropylmagnesium bromide / 2-methyltetrahydrofuran; tetrahydrofuran / 1 h / 0 °C

3.2: 72 h / 20 °C

4.1: Jones reagent / acetone / 3 h / 0 °C

5.1: potassium carbonate / acetonitrile / 5 h / 20 °C

With N-iodo-succinimide; Jones reagent; isopropylmagnesium bromide; potassium carbonate; hydrazine hydrate; In tetrahydrofuran; 2-methyltetrahydrofuran; ethanol; water; acetone; acetonitrile;