Acetamide, 2,2,2-trifluoro-N-phenoxy-

Base Information

Chemical Name:Acetamide, 2,2,2-trifluoro-N-phenoxy-
CAS No.:96661-31-3
Molecular Formula:C8H6F3NO2
Molecular Weight:205.136
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetamide, 2,2,2-trifluoro-N-phenoxy-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Acetamide, 2,2,2-trifluoro-N-phenoxy-

There total 1 articles about Acetamide, 2,2,2-trifluoro-N-phenoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-80-6
phenylboronic acid

: 96661-31-3
2,2,2-trifluoro-N-phenoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(II) acetate monohydrate; pyridine / 1,2-dichloro-ethane / Inert atmosphere; Molecular sieve

2.1: hydrazine hydrate / dichloromethane / Inert atmosphere

2.2: Inert atmosphere

With pyridine; copper(II) acetate monohydrate; hydrazine hydrate; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.202011140

Reference yield: 49.0%

: 141-32-2,9003-49-0
acrylic acid n-butyl ester

: 96661-31-3
2,2,2-trifluoro-N-phenoxyacetamide

: (+)-butyl (S)-3-(2-hydroxyphenyl)-2-(2,2,2-trifluoroacetamido)propanoate

Guidance literature:: 2,2,2-trifluoro-N-phenoxyacetamide; With C₃₃H₂₉CoI₂O₃; cesium acetate; silver trifluoromethanesulfonate; at 23 ℃; for 0.0166667h; Inert atmosphere; Glovebox; Molecular sieve; Sealed tube;

acrylic acid n-butyl ester; at 0 ℃; for 14h; enantioselective reaction; Inert atmosphere; Glovebox; Molecular sieve; Sealed tube;
DOI:10.1002/anie.202011140

Reference yield:

: 96661-31-3
2,2,2-trifluoro-N-phenoxyacetamide

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 92-69-3
4-Phenylphenol

: 90-43-7,287950-96-3
2-Phenylphenol

Guidance literature:: trifluorormethanesulfonic acid; trifluoroacetic acid; for 2h; Product distribution; Ambient temperature;
DOI:10.1016/S0040-4020(01)91336-5