1,2-Diphosphete, 3,4-bis(1,1-dimethylethyl)-1,2-dihydro-1-phenyl-, lithium salt

Base Information

Chemical Name:1,2-Diphosphete, 3,4-bis(1,1-dimethylethyl)-1,2-dihydro-1-phenyl-, lithium salt
CAS No.:96693-31-1
Molecular Formula:C16H24P2.Li
Molecular Weight:284.247
Hs Code.:

Synonyms:

Suppliers and Price of 1,2-Diphosphete, 3,4-bis(1,1-dimethylethyl)-1,2-dihydro-1-phenyl-, lithium salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1,2-Diphosphete, 3,4-bis(1,1-dimethylethyl)-1,2-dihydro-1-phenyl-, lithium salt

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-Diphosphete, 3,4-bis(1,1-dimethylethyl)-1,2-dihydro-1-phenyl-, lithium salt

There total 1 articles about 1,2-Diphosphete, 3,4-bis(1,1-dimethylethyl)-1,2-dihydro-1-phenyl-, lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75600-54-3,96693-29-7
1,2-diphenyl-3,4-di-t-butyldiphosphete

: 591-51-5
phenyllithium

: 96693-31-1
(2-phenyl-3,4-di-tert-butyl-1,2-diphosphetenyl)lithium

Guidance literature:: With lithium; In tetrahydrofuran; Product distribution; Ambient temperature;
DOI:10.1039/c39840001707

Reference yield: 62.0%

: 96693-31-1
(2-phenyl-3,4-di-tert-butyl-1,2-diphosphetenyl)lithium

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: {Mo(CO)5(C₆H₅(PC(C(CH₃)3))2CH₃)}

Guidance literature:: With methyl iodide; In tetrahydrofuran; under Ar; addn. of Mo hexacarbonyl to soln. of Li-compound; stirring at room temp. for 4h; addn. of 1 equivalent methyl iodide; evapn. of solvent; chromy. (silica gel, eluent: hexane-toluene 80:20); monitoring by NMR; elem. anal.;

Reference yield: 53.0%

: 14040-11-0
tungsten hexacarbonyl

: 96693-31-1
(2-phenyl-3,4-di-tert-butyl-1,2-diphosphetenyl)lithium

: {W(CO)5(C₆H₅(PC(C(CH₃)3))2CH₃)}

Guidance literature:: With methyl iodide; In tetrahydrofuran; under Ar; addn. of Mo hexacarbonyl to soln. of Li-compound; stirring at room temp. for 4h; addn. of 1 equivalent methyl iodide; evapn. of solvent; chromy. (silica gel, eluent: hexane-toluene 80:20); monitoring by NMR; elem. anal.;