4-Methyl-4',5'-benzo-8-azapsoralen

Base Information

Chemical Name:4-Methyl-4',5'-benzo-8-azapsoralen
CAS No.:120483-03-6
Molecular Formula:C₁₅H₉NO₃
Molecular Weight:251.241
Hs Code.:
DSSTox Substance ID:DTXSID20152878
Wikidata:Q83019653

Synonyms:4-Methyl-4',5'-benzo-8-azapsoralen;120483-03-6;DTXSID20152878

Suppliers and Price of 4-Methyl-4',5'-benzo-8-azapsoralen

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-Methyl-4',5'-benzo-8-azapsoralen

Chemical Property:

Vapor Pressure:4.27E-09mmHg at 25°C
Boiling Point:472.4°Cat760mmHg
Flash Point:239.5°C
Density:1.4g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:251.058243149
Heavy Atom Count:19
Complexity:433

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=O)OC2=NC3=C(C=C12)C4=CC=CC=C4O3

Technology Process of 4-Methyl-4',5'-benzo-8-azapsoralen

There total 4 articles about 4-Methyl-4',5'-benzo-8-azapsoralen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 120483-01-4
4-methyl-6,7,8,9-tetrahydrobenzofuro<2,3-e>pyrano<2,3-b>pyridin-2-one

: 120483-03-6
4-methylbenzofuro<2,3-e>pyrano<2,3-b>pyridin-2-one

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 48h; Heating;

Reference yield:

: 120482-92-0
4-methyl-7-(2'-oxocyclohexyloxy)pyrano<2,3-b>pyridin-2-one

: 120483-03-6
4-methylbenzofuro<2,3-e>pyrano<2,3-b>pyridin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / 5percent KOH / ethanol / 1 h / Heating

2: 21 percent / DDQ / toluene / 48 h / Heating

With potassium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; toluene;

Reference yield:

: 822-87-7
2-Chlorocyclohexanone

: 120483-03-6
4-methylbenzofuro<2,3-e>pyrano<2,3-b>pyridin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / K₂CO₃ / acetone / 240 h / Heating

2: 41 percent / 5percent KOH / ethanol / 1 h / Heating

3: 21 percent / DDQ / toluene / 48 h / Heating

With potassium hydroxide; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; acetone; toluene;