N-(2-Methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide

Base Information

Chemical Name:N-(2-Methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide
CAS No.:97847-83-1
Molecular Formula:C22H24NOP
Molecular Weight:349.412
Hs Code.:
DSSTox Substance ID:DTXSID10540503
Nikkaji Number:J2.299.252J

Synonyms:97847-83-1;DTXSID10540503;N-(2-Methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide

Suppliers and Price of N-(2-Methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-Methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:349.159551387
Heavy Atom Count:25
Complexity:409

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C(C1=CC=CC=C1)NP(=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of N-(2-Methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide

There total 2 articles about N-(2-Methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 625-81-0
diisopropyl zinc

: 98837-46-8
N-benzylidenediphenylphosphinamide

: 97847-83-1
N-(2-methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide

Guidance literature:: bis(acetylacetonate)nickel(II); In toluene; acetonitrile; at 0 ℃; for 1h;
DOI:10.1016/j.tet.2006.11.056

Reference yield:

: 1499-21-4
Diphenylphosphinic chloride

: 97847-83-1
N-(2-methyl-1-phenylpropyl)-P,P-diphenylphosphinic amide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / triethylamine / CH₂Cl₂ / 2.5 h / -5 °C

2: 1.) Mg / 1.) THF, 2.) diglyme, 120-130 deg C, reflux 3h

With magnesium; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)98444-2