Benzenemethanol, a-[[bis(1-methylethyl)amino]methyl]-4-hydroxy-2,3-dimethyl-, hydrochloride

Base Information

Chemical Name:Benzenemethanol, a-[[bis(1-methylethyl)amino]methyl]-4-hydroxy-2,3-dimethyl-, hydrochloride
CAS No.:97900-40-8
Molecular Formula:C16H27NO2.ClH
Molecular Weight:301.857
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanol, a-[[bis(1-methylethyl)amino]methyl]-4-hydroxy-2,3-dimethyl-, hydrochloride

Chemical Property:

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Technology Process of Benzenemethanol, a-[[bis(1-methylethyl)amino]methyl]-4-hydroxy-2,3-dimethyl-, hydrochloride

There total 6 articles about Benzenemethanol, a-[[bis(1-methylethyl)amino]methyl]-4-hydroxy-2,3-dimethyl-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

: 97888-88-5
2-diisopropylamino-1-(4-benzyloxy-2,3-dimethylphenyl)-ethanol hydrochloride

: 97900-40-8
2-diisopropylamino-1-(4-hydroxy-2,3-dimethylphenyl)-ethanol hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;

Reference yield:

: 526-75-0
2,3-Dimethylphenol

: 97900-40-8
2-diisopropylamino-1-(4-hydroxy-2,3-dimethylphenyl)-ethanol hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 27.5 percent / aluminium chloride / 1,2-dichloro-ethane / 4 h / 20 °C

2: 67 percent / sodium hydroxide, sodium iodide / H₂O; ethanol / 5 h / Heating

3: 55 percent / 48percent hydrogen bromide, bromine / methanol / 30 °C

4: 42.6 percent / ethanol / 3 h / Heating

5: 1.) sodium tetrahydridoborate, 2.) 20percent hydrogen chloride / 1.) ethanol, 0 deg C, 5 h 30 min, 2.) ethanol

6: 91.5 percent / H₂ / Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; hydrogen bromide; hydrogen; bromine; sodium iodide; palladium on activated charcoal; In methanol; ethanol; water; 1,2-dichloro-ethane;

Reference yield:

: 5384-57-6
4-hydroxy-2,3-dimethylacetophenone

: 97900-40-8
2-diisopropylamino-1-(4-hydroxy-2,3-dimethylphenyl)-ethanol hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 67 percent / sodium hydroxide, sodium iodide / H₂O; ethanol / 5 h / Heating

2: 55 percent / 48percent hydrogen bromide, bromine / methanol / 30 °C

3: 42.6 percent / ethanol / 3 h / Heating

4: 1.) sodium tetrahydridoborate, 2.) 20percent hydrogen chloride / 1.) ethanol, 0 deg C, 5 h 30 min, 2.) ethanol

5: 91.5 percent / H₂ / Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; hydrogen bromide; hydrogen; bromine; sodium iodide; palladium on activated charcoal; In methanol; ethanol; water;