2-(Cyclohexen-1-yl)-1-ethynyl-2-methylcyclohexan-1-ol

Base Information

Chemical Name:2-(Cyclohexen-1-yl)-1-ethynyl-2-methylcyclohexan-1-ol
CAS No.:97937-27-4
Molecular Formula:C₁₅H₂₂O
Molecular Weight:218.339
Hs Code.:
DSSTox Substance ID:DTXSID20560171

Synonyms:97937-27-4;DTXSID20560171;2-Ethynyl-1-methyl[[1,1'-bi(cyclohexan)]-1'-en]-2-ol

Suppliers and Price of 2-(Cyclohexen-1-yl)-1-ethynyl-2-methylcyclohexan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(Cyclohexen-1-yl)-1-ethynyl-2-methylcyclohexan-1-ol

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:218.167065321
Heavy Atom Count:16
Complexity:346

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCCCC1(C#C)O)C2=CCCCC2

Technology Process of 2-(Cyclohexen-1-yl)-1-ethynyl-2-methylcyclohexan-1-ol

There total 3 articles about 2-(Cyclohexen-1-yl)-1-ethynyl-2-methylcyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 54030-81-8
2-methyl-2-(cyclohexen-1'-yl)-cyclohexanone

: 70277-75-7
lithium acetylide

: 97937-27-4,126560-04-1
(1R,2S)-2-Ethynyl-1-methyl-bicyclohexyl-1'-en-2-ol

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/S0040-4020(96)00341-9

Reference yield:

: 1011-12-7
2-cyclohexylidenecyclohexanone

: 97937-27-4,126560-04-1
(1R,2S)-2-Ethynyl-1-methyl-bicyclohexyl-1'-en-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / t-BuOK / 2-methyl-propan-2-ol / 6 h / Ambient temperature

2: 90 percent / tetrahydrofuran / 2 h / -78 °C

With potassium tert-butylate; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/S0040-4020(96)00341-9

Reference yield:

: 1502-22-3
2-(1-cyclohexenyl)cyclohexanone

: 97937-27-4,126560-04-1
(1R,2S)-2-Ethynyl-1-methyl-bicyclohexyl-1'-en-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / t-BuOK / 14 h / Ambient temperature

2: 86 percent / tetrahydrofuran

With potassium tert-butylate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)99379-1