Bis(2,4-di-tert-butylphenyl) pentaerythritol diphosphate

Base Information

Chemical Name:Bis(2,4-di-tert-butylphenyl) pentaerythritol diphosphate
CAS No.:97994-11-1
Molecular Formula:C33H50O8P2
Molecular Weight:636.703
Hs Code.:
UNII:AX3T512R13
DSSTox Substance ID:DTXSID801043497
Nikkaji Number:J2.546.511C,J547.103F
Wikidata:Q27274167

Synonyms:97994-11-1;XR 2502;XR-2502;Bis(2,4-di-tert- butylphenyl) pentaerythritol diphosphate;UNII-AX3T512R13;AX3T512R13;S 9928;S-9928;2,4,8,10-Tetraoxa-3,9-diphosphaspiro(5.5)undecane, 3,9-bis(2,4-bis(1,1-dimethylethyl)phenoxy)-, 3,9-dioxide;SCHEMBL14566899;DTXSID801043497;EX-A7290;NS00127917;Q27274167;PENTAERYTHRITYL BIS(2,4-DI-TERT-BUTYLPHENYL PHOSPHATE);3,9-Bis(2,4-di-tert-butylphenoxy)-2,4,8,10-tetraoxa-3,9-diphosphaspiro[5.5]undecane 3,9-dioxide

Suppliers and Price of Bis(2,4-di-tert-butylphenyl) pentaerythritol diphosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of Bis(2,4-di-tert-butylphenyl) pentaerythritol diphosphate

Chemical Property:

XLogP3:8.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:8
Exact Mass:636.29809254
Heavy Atom Count:43
Complexity:951

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=C(C=C1)OP2(=O)OCC3(CO2)COP(=O)(OC3)OC4=C(C=C(C=C4)C(C)(C)C)C(C)(C)C)C(C)(C)C

Technology Process of Bis(2,4-di-tert-butylphenyl) pentaerythritol diphosphate

There total 4 articles about Bis(2,4-di-tert-butylphenyl) pentaerythritol diphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 26741-53-7,87498-44-0
3,9-bis(2,4-di-tert-butylphenoxy)-2,4,8,10-tetra-oxa-3,9-diphosphaspiro[5.5]-undecane

: 97994-11-1
3,9-bis[2,4-di-(tert-butyl)phenoxy]-2,4,8,10-tetraoxa-3λ⁵,9λ⁵-diphosphaspiro[5.5]undecane-3,9-dioxide

Guidance literature:: With dimethyl sulfoxide; In dichloromethane; at -80 ℃; for 2h;
DOI:10.14233/ajchem.2013.14068

Reference yield:

: 714-87-4
3,9-dichloro-2,4,8,10-tetraoxa-3,9-diphospaspiro <5,5>undecane 3,9-dioxide

: 96-76-4
2,4-di-tert-Butylphenol

: 97994-11-1
3,9-bis[2,4-di-(tert-butyl)phenoxy]-2,4,8,10-tetraoxa-3λ⁵,9λ⁵-diphosphaspiro[5.5]undecane-3,9-dioxide

Guidance literature:: With triethylamine; In benzene;
DOI:10.1002/mrc.1260230215

Reference yield:

: 115-77-5
Pentaerythritol

: 97994-11-1
3,9-bis[2,4-di-(tert-butyl)phenoxy]-2,4,8,10-tetraoxa-3λ⁵,9λ⁵-diphosphaspiro[5.5]undecane-3,9-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; phosphorus trichloride / toluene / 1 h / 5 °C

1.2: 5 h / Reflux

2.1: dimethyl sulfoxide / dichloromethane / 2 h / -80 °C

With dimethyl sulfoxide; triethylamine; phosphorus trichloride; In dichloromethane; toluene;
DOI:10.14233/ajchem.2013.14068