Benzene, 2-nitro-1,3-bis(phenylthio)-

Base Information

Chemical Name:Benzene, 2-nitro-1,3-bis(phenylthio)-
CAS No.:98119-89-2
Molecular Formula:C18H13NO2S2
Molecular Weight:339.43100
Hs Code.:

Synonyms:(2-nitro-1,3-phenylene)bis(phenylsulfane);2,6-bis(phenylsulfanyl)nitrobenzene;Benzene,2-nitro-1,3-bis(phenylthio);

Suppliers and Price of Benzene, 2-nitro-1,3-bis(phenylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Nitro-1,3-bis(phenylthio)benzene
2.5g
$ 545.00

TRC
2-Nitro-1,3-bis(phenylthio)benzene
1g
$ 240.00

TRC
2-Nitro-1,3-bis(phenylthio)benzene
250mg
$ 85.00

Total 0 raw suppliers

Chemical Property of Benzene, 2-nitro-1,3-bis(phenylthio)-

Chemical Property:

Boiling Point:468.9±40.0 °C(Predicted)
PSA：96.42000
Density:1.36±0.1 g/cm3(Predicted)
LogP:6.42040

Purity/Quality:: 2-Nitro-1,3-bis(phenylthio)benzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 2-Nitro-1,3-bis(phenylthio)benzene is an intermediate in the synthesis of 9-Chloro Quetiapine (C366040). 9-Chloro Quetiapine is an impurity of Quetiapine hemifumarate (Q510000), a dibenzothiazepine antipsychotic medication used in the treatment of schizophrenia.

Technology Process of Benzene, 2-nitro-1,3-bis(phenylthio)-

There total 2 articles about Benzene, 2-nitro-1,3-bis(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 19064-24-5
2,6-difluoro-1-nitrobenzene

: 108-98-5
thiophenol

: 98119-89-2
(2-nitro-1,3-phenylene)bis(phenylsulfane)

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 25 ℃;
DOI:10.1002/cmdc.201000420

Reference yield: 77.0%

: 601-88-7
2,6-dichloronitrobenzene

: 108-98-5
thiophenol

: 98119-89-2
(2-nitro-1,3-phenylene)bis(phenylsulfane)

Guidance literature:: thiophenol; With sodium; In ethanol; at 20 ℃; for 0.5h; Inert atmosphere;

2,6-dichloronitrobenzene; In ethanol; for 21h; Inert atmosphere; Reflux;
DOI:10.1002/cplu.201300428