Benzamide, 6-amino-2,3-dimethoxy-N-(7-methoxynaphtho[2,3-d]-1,3-dioxol-5-yl)-N- methyl-

Base Information

Chemical Name:Benzamide, 6-amino-2,3-dimethoxy-N-(7-methoxynaphtho[2,3-d]-1,3-dioxol-5-yl)-N- methyl-
CAS No.:98263-32-2
Molecular Formula:C22H22N2O6
Molecular Weight:410.426
Hs Code.:

Synonyms:

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Chemical Property of Benzamide, 6-amino-2,3-dimethoxy-N-(7-methoxynaphtho[2,3-d]-1,3-dioxol-5-yl)-N- methyl-

Chemical Property:

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Technology Process of Benzamide, 6-amino-2,3-dimethoxy-N-(7-methoxynaphtho[2,3-d]-1,3-dioxol-5-yl)-N- methyl-

There total 11 articles about Benzamide, 6-amino-2,3-dimethoxy-N-(7-methoxynaphtho[2,3-d]-1,3-dioxol-5-yl)-N- methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 98263-31-1
N-(3-methoxy-6,7-methylenedioxynaphth-1-yl)-N-methylamide of 2,3-dimethoxy-6-nitrobenzoic acid

: 98263-32-2
N-(3-methoxy-6,7-methylenedioxynaphth-1-yl)-N-methylamide of 6-amino-2,3-dimethoxybenzoic acid

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethanol; for 6h;

Reference yield:

: 98263-23-1
ethyl 3-hydroxy-6,7-methylenedioxy-1-naphthoate

: 98263-32-2
N-(3-methoxy-6,7-methylenedioxynaphth-1-yl)-N-methylamide of 6-amino-2,3-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: 75 percent / diethyl ether; methanol / 20 h

2: 88 percent / 10percent aq. KOH / ethanol / 5 h / Heating

3: 26.6 g / SOCl₂ / 2 h / Heating

4: 97 percent / NaN₃ / H₂O; dioxane / 0.5 h / 4 °C

5: 66 percent / benzene / 1 h / Heating

6: 82 percent / LiAlH₄ / benzene; diethyl ether / 1 h / Heating

7: 84.5 percent / K₂CO₃ / diethyl ether / 3 h / Heating

8: 93.5 percent / H₂ / 5percent Pd/CaCO₃ / ethanol / 6 h

With potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; sodium azide; hydrogen; potassium carbonate; Lindlar's catalyst; In 1,4-dioxane; methanol; diethyl ether; ethanol; water; benzene;

Reference yield:

: 98263-25-3
ethyl 3-methoxy-6,7-methylenedioxy-1-naphthoate

: 98263-32-2
N-(3-methoxy-6,7-methylenedioxynaphth-1-yl)-N-methylamide of 6-amino-2,3-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / 10percent aq. KOH / ethanol / 5 h / Heating

2: 26.6 g / SOCl₂ / 2 h / Heating

3: 97 percent / NaN₃ / H₂O; dioxane / 0.5 h / 4 °C

4: 66 percent / benzene / 1 h / Heating

5: 82 percent / LiAlH₄ / benzene; diethyl ether / 1 h / Heating

6: 84.5 percent / K₂CO₃ / diethyl ether / 3 h / Heating

7: 93.5 percent / H₂ / 5percent Pd/CaCO₃ / ethanol / 6 h

With potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; sodium azide; hydrogen; potassium carbonate; Lindlar's catalyst; In 1,4-dioxane; diethyl ether; ethanol; water; benzene;