Technology Process of heptatetracontane, 24,24-diethyl-19,29-dioctadecyl-
There total 8 articles about heptatetracontane, 24,24-diethyl-19,29-dioctadecyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: (i) N2H4*H2O, triethylene glycol, (ii) KOH
2: Na
2(OCH2CH2OMe)2> / benzene / Heating
3: H2SO4, aq. HBr / 6 h / Heating
4: (i) NaOEt, EtOH, (ii) /BRN= 2425374/, (iii) KOH, (iv) (heating)
5: TsOH / CCl4 / Heating
6: (i) Mg, ether, BrCH2CH2Br, (ii) /BRN= 2462934/
7: (i) TsOH, benzene, (ii) H2, Pt-C, cyclohexane
With
sulfuric acid; hydrogen bromide; toluene-4-sulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrachloromethane; benzene;
DOI:10.1002/hlca.19790620743
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Na
2(OCH2CH2OMe)2> / benzene / Heating
2: H2SO4, aq. HBr / 6 h / Heating
3: (i) NaOEt, EtOH, (ii) /BRN= 2425374/, (iii) KOH, (iv) (heating)
4: TsOH / CCl4 / Heating
5: (i) Mg, ether, BrCH2CH2Br, (ii) /BRN= 2462934/
6: (i) TsOH, benzene, (ii) H2, Pt-C, cyclohexane
With
sulfuric acid; hydrogen bromide; toluene-4-sulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrachloromethane; benzene;
DOI:10.1002/hlca.19790620743
- Guidance literature:
-
Multi-step reaction with 5 steps
1: H2SO4, aq. HBr / 6 h / Heating
2: (i) NaOEt, EtOH, (ii) /BRN= 2425374/, (iii) KOH, (iv) (heating)
3: TsOH / CCl4 / Heating
4: (i) Mg, ether, BrCH2CH2Br, (ii) /BRN= 2462934/
5: (i) TsOH, benzene, (ii) H2, Pt-C, cyclohexane
With
sulfuric acid; hydrogen bromide; toluene-4-sulfonic acid;
In
tetrachloromethane;
DOI:10.1002/hlca.19790620743