[2.2.2.2](1,2,3,5)Cyclophane

Base Information

Chemical Name:[2.2.2.2](1,2,3,5)Cyclophane
CAS No.:61477-04-1
Molecular Formula:C20H20
Molecular Weight:260.3728
Hs Code.:2902909090
DSSTox Substance ID:DTXSID00210440
Nikkaji Number:J18.063G
Wikidata:Q83085157
Mol file:61477-04-1.mol

Synonyms:[2.2.2.2](1,2,3,5)Cyclophane;61477-04-1;(2.2.2.2)(1,2,3,5)Cyclophane;DTXSID00210440

Suppliers and Price of [2.2.2.2](1,2,3,5)Cyclophane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of [2.2.2.2](1,2,3,5)Cyclophane

Chemical Property:

Vapor Pressure:3.39E-05mmHg at 25°C
Boiling Point:365°Cat760mmHg
Flash Point:188.4°C
PSA：0.00000
Density:1.161g/cm³
LogP:3.76760
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:260.156500638
Heavy Atom Count:20
Complexity:308

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CC3=C4CCC5=C(CC3)C=C1C=C5CCC4=C2

Technology Process of [2.2.2.2](1,2,3,5)Cyclophane

There total 4 articles about [2.2.2.2](1,2,3,5)Cyclophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61477-01-8
(13-Hydroxymethyl-12,16-dimethyl-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl)-methanol

: 61477-04-1
(1,2,3,5)tetra[2.2]cyclophane

Guidance literature:: Multi-step reaction with 2 steps

1: MnO₂

2: (i) TsNHNH₂, aq. HCl, (ii) NaOMe, (iii) (UV-irradiation)

With manganese(IV) oxide;

Reference yield:

: 61477-00-7
13,16-Bis-chloromethyl-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹²⁾,4⁽¹⁶⁾,5,7⁽¹⁵⁾,10,13-hexaene-5,12-dicarboxylic acid dimethyl ester

: 61477-04-1
(1,2,3,5)tetra[2.2]cyclophane

Guidance literature:: Multi-step reaction with 3 steps

1: iBu₂AlH

2: MnO₂

3: (i) TsNHNH₂, aq. HCl, (ii) NaOMe, (iii) (UV-irradiation)

With manganese(IV) oxide; diisobutylaluminium hydride;

Reference yield:

: 53922-65-9,53990-90-2,189224-11-1
<2.2>Paracyclophan-4,13-dicarbonsaeure-dimethylester

: 61477-04-1
(1,2,3,5)tetra[2.2]cyclophane

Guidance literature:: Multi-step reaction with 4 steps

1: AlCl₃

2: iBu₂AlH

3: MnO₂

4: (i) TsNHNH₂, aq. HCl, (ii) NaOMe, (iii) (UV-irradiation)

With manganese(IV) oxide; aluminium trichloride; diisobutylaluminium hydride;