(1,2,4)Triazolo(1,5-a)pyrimidine-2-sulfonamide, N-(2,6-dichlorophenyl)-5-methyl-

Base Information

• Chemical Name: (1,2,4)Triazolo(1,5-a)pyrimidine-2-sulfonamide, N-(2,6-dichlorophenyl)-5-methyl-
• CAS No.: 98967-26-1
• Molecular Formula: C12H9Cl2N5O2S
• Molecular Weight: 358.208

Synonyms:(1,2,4)Triazolo(1,5-a)pyrimidine-2-sulfonamide, N-(2,6-dichlorophenyl)-5-methyl-;98967-26-1;SCHEMBL8358999

Chemical Property of (1,2,4)Triazolo(1,5-a)pyrimidine-2-sulfonamide, N-(2,6-dichlorophenyl)-5-methyl-

Chemical Property:

• XLogP3: 2.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 356.9854011
• Heavy Atom Count: 22
• Complexity: 492

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC=NC2=NC(=NN12)S(=O)(=O)NC3=C(C=CC=C3Cl)Cl

Technology Process of (1,2,4)Triazolo(1,5-a)pyrimidine-2-sulfonamide, N-(2,6-dichlorophenyl)-5-methyl-

There total 1 articles about (1,2,4)Triazolo(1,5-a)pyrimidine-2-sulfonamide, N-(2,6-dichlorophenyl)-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

5-methyl-1,2,4-triazolo[1,5-a]pyrimidine-2-sulfonyl chloride (98165-60-7) + 2,6-Dichloroaniline (608-31-1) → 5-methyl-N-(2,6-dichlorophenyl)-1,2,4-triazolo[1,5-a]-pyrimidine-2-sulfonamide (98967-26-1)

Guidance literature:

With pyridine; dimethyl sulfoxide; In hexane; dichloromethane; acetonitrile;

Reference yield:

N-Bromosuccinimide (128-08-5) + 5-methyl-N-(2,6-dichlorophenyl)-1,2,4-triazolo[1,5-a]-pyrimidine-2-sulfonamide (98967-26-1) → 6-bromo-5-methyl-N-(2,6-dichlorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine-2-sulfonamide

Guidance literature:

With acetic anhydride; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dichloromethane; acetic acid;

Reference yield:

5-methyl-N-(2,6-dichlorophenyl)-1,2,4-triazolo[1,5-a]-pyrimidine-2-sulfonamide (98967-26-1) + methane sulfonic acid → 5-methyl-N-(2,6-dichlorophenyl)-4,5,6,7-tetrahydro-1,2,4-triazolo[1,5-a]pyrimidine-2-sulfonamide

Guidance literature:

With sodium hydroxide; sodium borohydrid; In dimethyl sulfoxide;

upstream raw materials:

5-methyl-1,2,4-triazolo[1,5-a]pyrimidine-2-sulfonyl chloride

2,6-Dichloroaniline

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