3,5-Diethyl-2,6-dimethyl-1H,7H-pyrazolo[1,2-a]pyrazole-1,7-dione

Base Information

Chemical Name:3,5-Diethyl-2,6-dimethyl-1H,7H-pyrazolo[1,2-a]pyrazole-1,7-dione
CAS No.:99240-32-1
Molecular Formula:C12H16N2O2
Molecular Weight:220.271
Hs Code.:
DSSTox Substance ID:DTXSID10556700

Synonyms:99240-32-1;DTXSID10556700;3,5-Diethyl-2,6-dimethyl-1H,7H-pyrazolo[1,2-a]pyrazole-1,7-dione

Suppliers and Price of 3,5-Diethyl-2,6-dimethyl-1H,7H-pyrazolo[1,2-a]pyrazole-1,7-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 3,5-Diethyl-2,6-dimethyl-1H,7H-pyrazolo[1,2-a]pyrazole-1,7-dione

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:220.121177757
Heavy Atom Count:16
Complexity:406

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=C(C(=O)N2N1C(=C(C2=O)C)CC)C

Technology Process of 3,5-Diethyl-2,6-dimethyl-1H,7H-pyrazolo[1,2-a]pyrazole-1,7-dione

There total 1 articles about 3,5-Diethyl-2,6-dimethyl-1H,7H-pyrazolo[1,2-a]pyrazole-1,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.3%

: 88848-54-8
3-(1-Bromo-ethyl)-5-ethyl-2,6-dimethyl-pyrazolo[1,2-a]pyrazole-1,7-dione

: 99240-32-1
9,10-dioxa-syn-(ethyl,methyl)bimane

: 129065-57-2
9,10-dioxa-syn-(1-(phenylthio)ethyl,methyl)(ethyl,methyl)bimane

Guidance literature:: With sodium thiophenolate; In tetrahydrofuran; for 0.333333h; Ambient temperature;
DOI:10.1021/ja00176a034

Reference yield:

: 99240-32-1
9,10-dioxa-syn-(ethyl,methyl)bimane

: 102420-27-9
cis-9,10-dioxa-μ-(S)-syn-(methylmethylene,methyl)bimane

Guidance literature:: Multi-step reaction with 2 steps

1: bromine, NaHCO₃ / CH₂Cl₂ / 1 h

2: 21.5 percent / Na₂S / hexadecyltrimethylammonium bromide / CH₂Cl₂; H₂O / 7 h

With sodium sulfide; bromine; sodium hydrogencarbonate; cetyltrimethylammonim bromide; In dichloromethane; water;
DOI:10.1021/ja00275a046

Reference yield:

: 99240-32-1
9,10-dioxa-syn-(ethyl,methyl)bimane

: 102420-28-0
trans-μ-(S)-syn-(methylmethylene,methyl)bimane

Guidance literature:: Multi-step reaction with 2 steps

1: bromine, NaHCO₃ / CH₂Cl₂ / 1 h

2: 78.5 percent / Na₂S / hexadecyltrimethylammonium bromide / CH₂Cl₂; H₂O / 7 h

With sodium sulfide; bromine; sodium hydrogencarbonate; cetyltrimethylammonim bromide; In dichloromethane; water;
DOI:10.1021/ja00275a046