2,4-Piperidinedione, 1-(2-phenylethyl)-

Base Information

Chemical Name:2,4-Piperidinedione, 1-(2-phenylethyl)-
CAS No.:99539-57-8
Molecular Formula:C13H15NO2
Molecular Weight:217.268
Hs Code.:
DSSTox Substance ID:DTXSID20442443
Nikkaji Number:J754.193G
Wikidata:Q82259720

Synonyms:1-phenethylpiperidine-2,4-dione;2,4-Piperidinedione, 1-(2-phenylethyl)-;99539-57-8;SCHEMBL10750812;1-phenethyl-2,4-dioxopiperidine;DTXSID20442443;NHNODOKVRYUPOT-UHFFFAOYSA-N;AKOS018073411

Suppliers and Price of 2,4-Piperidinedione, 1-(2-phenylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 2,4-Piperidinedione, 1-(2-phenylethyl)-

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:217.110278721
Heavy Atom Count:16
Complexity:269

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN(C(=O)CC1=O)CCC2=CC=CC=C2

Technology Process of 2,4-Piperidinedione, 1-(2-phenylethyl)-

There total 5 articles about 2,4-Piperidinedione, 1-(2-phenylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 182559-05-3
2,4-Dioxo-1-phenethyl-piperidine-3-carboxylic acid methyl ester

: 99539-57-8
1-phenethyl-2,4-dioxopiperidine

Guidance literature:: With oxalic acid; Heating;
DOI:10.1039/P19960002041

Reference yield: 86.4%

: 99539-57-8
1-phenethyl-2,4-dioxopiperidine

Guidance literature:

Reference yield:

: 40871-01-0
methyl 3-propionate

: 99539-57-8
1-phenethyl-2,4-dioxopiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 1 h / 160 - 170 °C

2: 85 percent / K₂CO₃, 18-crown-6 / toluene / 6 h / Heating

3: 90 percent / 10percent aq. oxalic acid / Heating

With 18-crown-6 ether; oxalic acid; potassium carbonate; In toluene;
DOI:10.1039/P19960002041