3-(1,3-Dioxolan-2-yl)-1-methylpiperidine

Base Information

Chemical Name:3-(1,3-Dioxolan-2-yl)-1-methylpiperidine
CAS No.:99803-15-3
Molecular Formula:C9H17NO2
Molecular Weight:171.23700
Hs Code.:2933399090
European Community (EC) Number:873-610-5
Mol file:99803-15-3.mol

Synonyms:3-(1,3-dioxolan-2-yl)-1-methylpiperidine;99803-15-3;Piperidine, 3-(1,3-dioxolan-2-yl)-1-methyl-;AKOS024463578;AM10503;EN300-74759;Z1091752556

Suppliers and Price of 3-(1,3-Dioxolan-2-yl)-1-methylpiperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-(1,3-Dioxolan-2-yl)-1-methylpiperidine
25mg
$ 45.00

Medical Isotopes, Inc.
3-(1,3-dioxolan-2-yl)-1-methylpiperidine 95%
1 g
$ 800.00

Crysdot
3-(1,3-Dioxolan-2-yl)-1-methylpiperidine 95+%
1g
$ 523.00

Chemenu
3-(1,3-dioxolan-2-yl)-1-methylpiperidine 95%
1g
$ 489.00

Alichem
3-(1,3-Dioxolan-2-yl)-1-methylpiperidine
1g
$ 434.66

Total 6 raw suppliers

Chemical Property of 3-(1,3-Dioxolan-2-yl)-1-methylpiperidine

Chemical Property:

Boiling Point:228.3±35.0 °C (760 mmHg)
PSA：21.70000
Density:1.057±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:0.63900
XLogP3:0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:171.125928785
Heavy Atom Count:12
Complexity:146

Purity/Quality:

97% ^*data from raw suppliers

3-(1,3-Dioxolan-2-yl)-1-methylpiperidine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCCC(C1)C2OCCO2

Technology Process of 3-(1,3-Dioxolan-2-yl)-1-methylpiperidine

There total 4 articles about 3-(1,3-Dioxolan-2-yl)-1-methylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 105688-89-9
5-(1,3-dioxolan-2-yl)-1-methyl-1,2,3,6-tetrahydropyridine

: 112391-02-3
3-(4-hydroxy-2-oxabutyl)-1-methylpiperidine

: 99803-15-3
3-(1,3-dioxolan-2-yl)-1-methylpiperidine

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; for 1h; under 2068.6 Torr; Ambient temperature;

Reference yield:

: 99803-14-2
3-(1,3-dioxolan-2-yl)-1-methylpyridinium iodide

: 99803-15-3
3-(1,3-dioxolan-2-yl)-1-methylpiperidine

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; for 20h; under 760 Torr; Ambient temperature;

Reference yield:

: 500-22-1
3-pyridinecarboxaldehyde

: 99803-15-3
3-(1,3-dioxolan-2-yl)-1-methylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / p-toluenesulfonic acid / 4 h / Heating

2: 90 percent / diethyl ether / 10 h / 10 - 15 °C

3: 54 percent / sodium borohydride / H₂O / 0.5 h / Ambient temperature

4: 30 percent / hydrogen / PtO₂ / methanol / 1 h / 2068.6 Torr / Ambient temperature

With sodium tetrahydroborate; hydrogen; toluene-4-sulfonic acid; platinum(IV) oxide; In methanol; diethyl ether; water;