PPQ-102

Base Information

• Chemical Name: PPQ-102
• CAS No.: 931706-15-9
• Molecular Formula: C26H22N4O3
• Molecular Weight: 438.48
• Mol file: 931706-15-9.mol

Synonyms:7.9-Dimethylxanthin;7,9-dimethoxy-5H-pyrido<3,2-c>azepine;7,9-dimethylxanthine;7,9-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purinium betaine;7,9-Dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-purinium-betain;7,9-dimethoxy-5H-pyrido<3,2-c>-azephine;3,9-dimethylxanthine;

Chemical Property of PPQ-102

Chemical Property:

• Melting Point: >300℃ (ethanol )
• Boiling Point: 648.7±65.0 °C(Predicted)
• PKA: 1.00±0.40(Predicted)
• PSA: 74.10000
• Density: 1.39±0.1 g/cm3(Predicted)
• LogP: 4.24920
• Storage Temp.: -20C

Purity/Quality:

99%, ^*data from raw suppliers

PPQ 102 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PPQ-102

There total 5 articles about PPQ-102 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

5-Methylfurfural (620-02-0) + 6-(2-aminophenyl)-1,3-dimethyl-5-phenyl-1H-pyrrolo[3,4-d]pyrimidine-2,4(3H,6H)-dione (433971-83-6) → PPQ-102 (931706-15-9)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; for 0.0833333h; Reflux;

DOI:10.1021/jm200505e

Reference yield:

1,3,6-trimethyluracil (13509-52-9) → PPQ-102 (931706-15-9)

Guidance literature:

Multi-step reaction with 4 steps

1: zinc(II) chloride / chlorobenzene / 3 h / Reflux

2: water; bromine / tetrachloromethane; dichloromethane / 0.17 h / 50 °C

3: ethanol / 1 h / Reflux

4: toluene-4-sulfonic acid / 1,2-dichloro-ethane / 0.08 h / Reflux

With water; bromine; toluene-4-sulfonic acid; zinc(II) chloride; In tetrachloromethane; ethanol; dichloromethane; 1,2-dichloro-ethane; chlorobenzene; 1: Friedel Crafts acylation;

DOI:10.1021/jm200505e

Reference yield:

6-Methyluracil (626-48-2) → PPQ-102 (931706-15-9)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium hydroxide / water / 72 h / 25 °C

2: zinc(II) chloride / chlorobenzene / 3 h / Reflux

3: water; bromine / tetrachloromethane; dichloromethane / 0.17 h / 50 °C

4: ethanol / 1 h / Reflux

5: toluene-4-sulfonic acid / 1,2-dichloro-ethane / 0.08 h / Reflux

With water; bromine; toluene-4-sulfonic acid; sodium hydroxide; zinc(II) chloride; In tetrachloromethane; ethanol; dichloromethane; water; 1,2-dichloro-ethane; chlorobenzene; 2: Friedel Crafts acylation;

DOI:10.1021/jm200505e

upstream raw materials:

5-Methylfurfural

6-(2-aminophenyl)-1,3-dimethyl-5-phenyl-1H-pyrrolo[3,4-d]pyrimidine-2,4(3H,6H)-dione

6-Methyluracil

1,3,6-trimethyluracil

Downstream raw materials:

N-(2-(1,3-dimethyl-2,4-dioxo-5-phenyl-3,4-dihydro-1H-pyrrolo[3,4-d]pyrimidin-6(2H)-yl)phenyl)-5-methylfuran-2-carboxamide

7,9-dimethyl-6-(5-methylfuran-2-yl)-5-nitroso-11-phenyl-5,6-dihydropyrimido[4',5':3,4]pyrrolo[1,2-a]quinoxaline-8,10(7H,9H)-dione

5-acetyl-7,9-dimethyl-6-(5-methylfuran-2-yl)-11-phenyl-5,6-dihydropyrimido[4',5':3,4]pyrrolo[1,2-a]quinoxaline-8,10(7H,9H)-dione

7,9-dimethyl-6-(5-methylfuran-2-yl)-5-(methylsulfonyl)-11-phenyl-5,6-dihydropyrimido[4',5':3,4]pyrrolo[1,2-a]quinoxaline-8,10(7H,9H)-dione

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 931706-15-9 PPQ-102

Send

Send

Metric Ton KG G Pound L ML

Send

Send