N-(methylthiomethoxy)-2-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(methylthiomethoxy)-2-nitrobenzenesulfonamide
CAS No.:869586-20-9
Molecular Formula:C8H10N2O5S2
Molecular Weight:278.31
Hs Code.:
DSSTox Substance ID:DTXSID90469167
Wikidata:Q82296763

Synonyms:N-(methylthiomethoxy)-2-nitrobenzenesulfonamide;869586-20-9;N-[(methylsulfanyl)methoxy]-2-nitrobenzene-1-sulfonamide;DTXSID90469167;FT-0740981

Suppliers and Price of N-(methylthiomethoxy)-2-nitrobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-(methylthiomethoxy)-2-nitrobenzenesulfonamide

Chemical Property:

Melting Point:131-133 °C(Solv: hexane (110-54-3); dichloromethane (75-09-2))
Boiling Point:425.1±55.0 °C(Predicted)
PSA：134.90000
Density:1.474±0.06 g/cm3(Predicted)
LogP:3.12010
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:278.00311377
Heavy Atom Count:17
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSCONS(=O)(=O)C1=CC=CC=C1[N+](=O)[O-]

Technology Process of N-(methylthiomethoxy)-2-nitrobenzenesulfonamide

There total 1 articles about N-(methylthiomethoxy)-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41108-16-1
O-<(methylthio)methyl>-hydroxylamine

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 869586-20-9
N-methylsulfanylmethoxy-2-nitrobenzenesulfonamide

Guidance literature:: With pyridine; In tetrahydrofuran; for 1h;
DOI:10.1021/ja055832h

Reference yield:

: 869586-20-9
N-methylsulfanylmethoxy-2-nitrobenzenesulfonamide

: 869586-56-1
N-[2-(6-bromo-5-methoxy-1H-indol-3-yl)ethyl]-N-methylsulfanyloxymethoxy-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / PPh₃; DEAD / benzene; toluene / 0.25 h / 20 °C

2: 97 percent / dimethyl sulfide; TFA / CH₂Cl₂ / 0.5 h / 20 °C

With dimethylsulfide; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In dichloromethane; toluene; benzene; 1: Mitsunobu reaction;
DOI:10.1021/ja055832h