2-N-boc-butane-1,2-diamine-hcl

Base Information

Chemical Name:2-N-boc-butane-1,2-diamine-hcl
CAS No.:138374-00-2
Molecular Formula:C9H20N2O2.HCL
Molecular Weight:224.7282
Hs Code.:2924199090
Mol file:138374-00-2.mol

Synonyms:2-N-Boc-butane-1,2-diamine-HCl;2-N-Boc-Butane-1,2-diaMine hydrochloride

Suppliers and Price of 2-N-boc-butane-1,2-diamine-hcl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(1-aminobutan-2-yl)carbamatehydrochloride 95+%
1g
$ 753.00

American Custom Chemicals Corporation
2-N-BOC-BUTANE-1,2-DIAMINE HYDROCHLORIDE 95.00%
5MG
$ 495.92

AK Scientific
2-N-Boc-Butane-1,2-diaminehydrochloride
10g
$ 2051.00

AK Scientific
2-N-Boc-Butane-1,2-diaminehydrochloride
5g
$ 1317.00

Total 17 raw suppliers

Chemical Property of 2-N-boc-butane-1,2-diamine-hcl

Chemical Property:

PSA：64.35000
LogP:3.14160

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl(1-aminobutan-2-yl)carbamatehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-N-boc-butane-1,2-diamine-hcl

There total 3 articles about 2-N-boc-butane-1,2-diamine-hcl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 138373-90-7
1-azido-2-(N-tert-butoxycarbonylamino)butane

: 138374-00-2
2-(N-tert-butoxycarbonyl)-1,2-diaminobutane hydrochloride

Guidance literature:: With chloroform; hydrogen; palladium on activated charcoal; In methanol; for 3h; under 1551.4 Torr; Ambient temperature;
DOI:10.1016/S0040-4020(01)91013-0

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 138374-00-2
2-(N-tert-butoxycarbonyl)-1,2-diaminobutane hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 1N aq. NaOH / CH₂Cl₂ / Ambient temperature

2: 82 percent / PPh₃, HN₃, diethyl azodicarboxylate / benzene; CH₂Cl₂ / Ambient temperature

3: 80 percent / H₂, CHCl₃ / 10percent Pd/C / methanol / 3 h / 1551.4 Torr / Ambient temperature

With sodium hydroxide; chloroform; tris-(2-chloro-ethyl)-amine; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In methanol; dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)91013-0

Reference yield:

: 193086-15-6
(1-(hydroxymethyl)propyl)carbamic acid tert-butyl ester

: 138374-00-2
2-(N-tert-butoxycarbonyl)-1,2-diaminobutane hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / PPh₃, HN₃, diethyl azodicarboxylate / benzene; CH₂Cl₂ / Ambient temperature

2: 80 percent / H₂, CHCl₃ / 10percent Pd/C / methanol / 3 h / 1551.4 Torr / Ambient temperature

With chloroform; tris-(2-chloro-ethyl)-amine; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In methanol; dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)91013-0