2,3-Bis(2,4,6-trimethylphenylimino)butane

Base Information

Chemical Name:2,3-Bis(2,4,6-trimethylphenylimino)butane
CAS No.:202277-65-4
Molecular Formula:C22H28N2
Molecular Weight:320.478
Hs Code.:
Mol file:202277-65-4.mol

Synonyms:2,3-Bis(2,4,6-trimethylphenylimino)butane;N,N'-(2E,3E)-butane-2,3-diylidenebis(2,4,6-trimethylaniline);

Suppliers and Price of 2,3-Bis(2,4,6-trimethylphenylimino)butane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,3-Bis(2,4,6-trimethylphenylimino)butane

Chemical Property:

Melting Point:187.4-188.2℃
PSA：24.72000
LogP:6.42200

Purity/Quality:: 99.3% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-Bis(2,4,6-trimethylphenylimino)butane

There total 1 articles about 2,3-Bis(2,4,6-trimethylphenylimino)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.8%

: 431-03-8
dimethylglyoxal

: 88-05-1
2,4,6-trimethylaniline

: 202277-65-4
1,2-bis[(2,4,6-trimethylphenyl)imino]-1,2-dimethylethane

Guidance literature:: With formic acid; In methanol; for 12h; Reflux; Inert atmosphere;
DOI:10.1016/S1872-2067(12)60625-1

Reference yield: 95.0%

: 202277-65-4
1,2-bis[(2,4,6-trimethylphenyl)imino]-1,2-dimethylethane

: 7789-46-0
iron(II) bromide

: C₂₂H₂₈Br₂FeN₂

Guidance literature:: In dichloromethane; at 20 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1016/j.poly.2016.02.020

Reference yield: 94.0%

: 115450-92-5
UI₃(tetrahydrofuran)4

: 202277-65-4
1,2-bis[(2,4,6-trimethylphenyl)imino]-1,2-dimethylethane

: ((CH₃)3C₆H₂NC(CH₃)C(CH₃)NC₆H₂(CH₃)3)2U(OC₄H₈)

Guidance literature:: With sodium; naphthalene; In tetrahydrofuran; ligand and catalytic amt. of naphthalene added to Na and THF; stirred for 1 h; added to U complex in THF; stirred for 3 h; solvent removed in vac.; taken up in ether-pentane; filtered through Celite; solvent removed from filtrate under vac.; recrystd. from pentane-ether at -35°C; elem. anal.;