2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone

Base Information

Chemical Name:2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
CAS No.:34051-37-1
Molecular Formula:C29H31NO6
Molecular Weight:489.55954
Hs Code.:
Mol file:34051-37-1.mol

Synonyms:2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone;

Suppliers and Price of 2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
50mg
$ 403.00

Usbiological
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
25mg
$ 403.00

TRC
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
500 mg
$ 970.00

TRC
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
50 mg
$ 120.00

Medical Isotopes, Inc.
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
500 mg
$ 1880.00

Biosynth Carbosynth
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
500 mg
$ 1205.00

Biosynth Carbosynth
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
100 mg
$ 364.00

Biosynth Carbosynth
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
50 mg
$ 200.50

Biosynth Carbosynth
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
25 mg
$ 110.00

Biosynth Carbosynth
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone
250 mg
$ 662.50

Total 7 raw suppliers

Chemical Property of 2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone

Chemical Property:

PSA：83.09000
LogP:4.19500
Solubility.:Acetone, Dichloromethane, DMSO,

Purity/Quality:

99% ^*data from raw suppliers

2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone

There total 12 articles about 2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 4171-79-3,121123-45-3,4171-72-6
N-((3R,4R,5S,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-2-hydroxy-tetrahydro-2H-pyran-3-yl)acetamide

: 34051-37-1
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lacton

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 0.833333h;
DOI:10.1002/hlca.19980810508

Reference yield: 90.0%

: 2-N-Acetylamino-3,4,6-tri-O-benzyl-2-deoxy-D-mannopyranose

: 34051-37-1
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lacton

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 3 A molecular sieve; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1080/07328309608005438

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 34051-37-1
2-Acetamido-3,4,6-tri-O-benzyl-2-deoxy-D-glucono-1,5-lacton

Guidance literature:: Multi-step reaction with 4 steps

1: BF₃*OEt₂ / 5 h / Heating

2: NaH / dimethylformamide / 2 h

3: 1.) t-BuOK; 2.) I₂ / 1.) DMSO, 60 deg C, 30 min; 2.) THF/H₂O, 30 min

4: 98 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.83 h

With boron trifluoride diethyl etherate; potassium tert-butylate; iodine; sodium hydride; Dess-Martin periodane; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19980810508