3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol

Base Information

• Chemical Name: 3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol
• CAS No.: 58261-88-4
• Molecular Formula: C30H47ClO3
• Molecular Weight: 491.14538
• Mol file: 58261-88-4.mol

Synonyms:3SS-ACETOXY-6A-CHLOROERGOSTA-7,22-DIEN-5A-OL;3Beta-Acetoxy-6Alpha-chloroergosta-7,22-dien-5Alpha-ol;3B-ACETOXY-6A-CHLOROERGOSTA-7,22-DIEN-5A-OL;

Chemical Property of 3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol

Chemical Property:

• PSA: 46.53000
• LogP: 7.31370
• Solubility.: Chloroform, Ethyl Acetate

Purity/Quality:

98%min ^*data from raw suppliers

3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol

There total 3 articles about 3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

ergosterol acetate (1108-03-8,2874-25-1,3957-39-9,57760-54-0,60018-28-2,78148-63-7,125225-12-9,2418-45-3) → 3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol (58261-88-4)

Guidance literature:

With chromyl chloride; acetyl chloride; In methyl cyclohexane; at -75 ℃; for 1h;

Reference yield:

chromyl chloride + ergosterol acetate (1108-03-8,2874-25-1,3957-39-9,57760-54-0,60018-28-2,78148-63-7,125225-12-9,2418-45-3) + acetonitrile (75-05-8,26809-02-9) → 3β-Acetoxy-6α-chloroergosta-7,22-dien-5α-ol (58261-88-4)

Guidance literature:

With hydrogenchloride; sodium borohydrid; In deoxygenated toluene; ethanol; dichloromethane; benzene;

Reference yield:

→ 6α-Chlor-5-hydroxy-5α-ergosta-7,22-dien-3β-yl-acetat (58261-88-4)

Guidance literature:

Aus Verb. I u. O2 in Gegenwart von TiCl4;

upstream raw materials:

ergosterol acetate

acetonitrile

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