2-[5-(Benzyloxy)-1H-indol-3-yl]-2-oxoacetic acid ,97%

Base Information

• Chemical Name: 2-[5-(Benzyloxy)-1H-indol-3-yl]-2-oxoacetic acid ,97%
• CAS No.: 101601-00-7
• Molecular Formula: C₁₇H₁₃NO₄
• Molecular Weight: 295.295
• Hs Code.: 29339900
• Mol file: 101601-00-7.mol

Synonyms:2-[5-(Benzyloxy)-1H-indol-3-yl]-2-oxoacetic acid ,97%;2-[5-(Benzyloxy)-1H-indol-3-yl]-2-oxoacetic acid

Chemical Property of 2-[5-(Benzyloxy)-1H-indol-3-yl]-2-oxoacetic acid ,97%

Chemical Property:

• PSA: 79.39000
• LogP: 3.01420

Purity/Quality:

97% ^*data from raw suppliers

5-Benzyloxyindole3-GlyoxylicAcid ^*data from reagent suppliers

Safty Information:

• Statements: 20/21/22-37/38-48
• Safety Statements: 7/8-22-26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 5-Benzyloxyindole 3-Glyoxylic Acid is a derivative of 5-Benzyloxyindole (B285949) and is used as a reagent in the synthesis of indole-3-acetic acids.

Technology Process of 2-[5-(Benzyloxy)-1H-indol-3-yl]-2-oxoacetic acid ,97%

There total 2 articles about 2-[5-(Benzyloxy)-1H-indol-3-yl]-2-oxoacetic acid ,97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[5-(benzyloxy)-1H-indol-3-yl]-2-oxoacetyl chloride (22424-61-9) → (5-benzyloxy-indol-3-yl)-glyoxylic acid (101601-00-7)

Guidance literature:

With potassium hydroxide;

Reference yield:

5-benzyloxy-1H-indole (1215-59-4) → (5-benzyloxy-indol-3-yl)-glyoxylic acid (101601-00-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / 0.33 h / 0 °C

2: sat. aq. NaHCO₃ / diethyl ether / 0.5 h / Heating

With sodium hydrogencarbonate; In diethyl ether;

DOI:10.1016/S0040-4039(00)76815-8

Reference yield:

(5-benzyloxy-indol-3-yl)-glyoxylic acid (101601-00-7) → 2-(5-benzyloxy-1H-indol-3-yl)acetic acid (4382-53-0)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 8 h / Heating

2: NaBH₄ / tetrahydrofuran / 10 h / Heating

With sodium tetrahydroborate; In tetrahydrofuran; methanol;

DOI:10.1016/S0040-4039(00)76815-8

upstream raw materials:

2-[5-(benzyloxy)-1H-indol-3-yl]-2-oxoacetyl chloride

5-benzyloxy-1H-indole

Downstream raw materials:

2-(5-benzyloxy-1H-indol-3-yl)acetic acid

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