3-Methylpentane-1,2,5-triol

Base Information

Chemical Name:3-Methylpentane-1,2,5-triol
CAS No.:72692-98-9
Molecular Formula:C₆H₁₄O₃
Molecular Weight:134.175
Hs Code.:
European Community (EC) Number:276-766-7
DSSTox Substance ID:DTXSID90993518
Nikkaji Number:J296.343D
Mol file:72692-98-9.mol

Synonyms:3-Methylpentane-1,2,5-triol;72692-98-9;EINECS 276-766-7;2,3-Dideoxy-3-methylpentitol;SCHEMBL9006500;DTXSID90993518

Suppliers and Price of 3-Methylpentane-1,2,5-triol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-Methylpentane-1,2,5-triol

Chemical Property:

Vapor Pressure:3.89E-05mmHg at 25°C
Boiling Point:314.8°C at 760 mmHg
Flash Point:159.5°C
PSA：60.69000
Density:1.11g/cm³
LogP:-0.64190
XLogP3:-0.6
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:134.094294304
Heavy Atom Count:9
Complexity:65.3

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CCO)C(CO)O

Technology Process of 3-Methylpentane-1,2,5-triol

There total 12 articles about 3-Methylpentane-1,2,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1395346-52-7
(4S,5S)-5-benzoyloxymethyl-3,4-dihydro-4-methylfuranone

: 1114-84-7,72692-98-9,73744-63-5
(2S,3R)-3-methyl-pentane-1,2,5-triol

Guidance literature:: (4S,5S)-5-benzoyloxymethyl-3,4-dihydro-4-methylfuranone; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

With water; ammonium chloride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2012.06.108

Reference yield:

: 114972-38-2,135006-18-7
(4S)-4-<(Z)-(2-carbomethoxy-1-methylethenyl)>-2,2-dimethyl-1,3-dioxolane

: 1114-84-7,72692-98-9,73744-63-5
(2S,3R)-3-methyl-pentane-1,2,5-triol

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / 3 N aq. HCl / tetrahydrofuran / 24 h / Ambient temperature

2: 100 percent / POCl₃ / 6 h / Ambient temperature

3: 100 percent / H₂ / 5percent Rh/Al₂O₃ / benzene / 4 h / 760 Torr

4: LiAlH₄ / diethyl ether / 1.5 h / 25 °C

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; trichlorophosphate; Rh/Al₂O₃; In tetrahydrofuran; diethyl ether; benzene;