N-Benzyloxycarbonyl Serotonin O-Sulfate

Base Information

• Chemical Name: N-Benzyloxycarbonyl Serotonin O-Sulfate
• CAS No.: 85376-01-8
• Molecular Formula: C18H18N2O7S
• Molecular Weight: 406.40972
• Mol file: 85376-01-8.mol

Synonyms:N-Benzyloxycarbonyl Serotonin O-Sulfate;[2-[5-(Sulfooxy)-1H-indol-3-yl]ethyl]carbaMic Acid (PhenylMethyl) Ester;[2-[5-(Sulfooxy)-1H-indol-3-yl]ethyl]carbaMic Acid Benzyl Ester;Z-Serotonin O-Sulfate

Chemical Property of N-Benzyloxycarbonyl Serotonin O-Sulfate

Chemical Property:

• PKA: -3.85±0.18(Predicted)
• PSA: 129.59000
• Density: 1.463±0.06 g/cm3(Predicted)
• LogP: 4.10360

Purity/Quality:

97% ^*data from raw suppliers

N-Benzyloxycarbonyl Serotonin O-Sulfate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Protected Serotonin derivative. N-Benzyloxycarbonyl Serotonin O-Sulfate is a protected Serotonin derivative, which is a useful building block in the synthesis of various pharmaceuticals.

Technology Process of N-Benzyloxycarbonyl Serotonin O-Sulfate

There total 3 articles about N-Benzyloxycarbonyl Serotonin O-Sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

N-Cbz-5-hydroxytryptamine (53157-50-9) → Z-Serotonin O-sulfate (85376-01-8)

Guidance literature:

With sulfur trioxide; In pyridine; for 19h; Ambient temperature;

DOI:10.1055/s-1983-30205

Reference yield:

serotonin creatinine sulfate (971-74-4) → Z-Serotonin O-sulfate (85376-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Na₂CO₃ / tetrahydrofuran; H₂O / 1 h / Ambient temperature

2: 83 percent / pyridine/sulfur trioxide complex / pyridine / 19 h / Ambient temperature

With pyridine; sulfur trioxide; sodium carbonate; In tetrahydrofuran; pyridine; water;

DOI:10.1055/s-1983-30205

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → Z-Serotonin O-sulfate (85376-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Na₂CO₃ / tetrahydrofuran; H₂O / 1 h / Ambient temperature

2: 83 percent / pyridine/sulfur trioxide complex / pyridine / 19 h / Ambient temperature

With pyridine; sulfur trioxide; sodium carbonate; In tetrahydrofuran; pyridine; water;

DOI:10.1055/s-1983-30205

upstream raw materials:

N-Cbz-5-hydroxytryptamine

serotonin creatinine sulfate

benzyl chloroformate

Downstream raw materials:

serotonin-O-sulfate

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