rac trans-3-Amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-4-carboxylic Acid

Base Information

• Chemical Name: rac trans-3-Amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-4-carboxylic Acid
• CAS No.: 15871-58-6
• Molecular Formula: C9H18N2O3
• Molecular Weight: 201.2429
• Mol file: 15871-58-6.mol

Synonyms:rac trans-3-Amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-4-carboxylic Acid;

Chemical Property of rac trans-3-Amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-4-carboxylic Acid

Chemical Property:

• PSA: 66.56000
• LogP: 0.87100

Purity/Quality:

99% ^*data from raw suppliers

ractrans-3-Amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-4-carboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: A spin-label.

Technology Process of rac trans-3-Amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-4-carboxylic Acid

There total 2 articles about rac trans-3-Amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-4-carboxylic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C44H39N2O6 → trans 3-(9-fluorenylmethyloxycarbonylamino)-1-oxyl-2,2,5,5,-tetramethylpyrrolidine-4-carboxylic acid (581085-80-5) + 4-amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-3-carboxylic acid (15871-58-6)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; methanol; at 50 ℃; for 3h; Title compound not separated from byproducts.;

DOI:10.1016/j.tet.2008.02.058

Reference yield:

→ 4-amino-1-oxyl-2,2,5,5-tetramethylpyrrolidine-3-carboxylic acid (15871-58-6)

Guidance literature:

4-Amino-2,2,5,5-tetramethyl-3-cyan-pyrrolidin-1-oxyl (vermutl. trans), aq. Ba(OH)2 (120grad);

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