5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam

Base Information

Chemical Name:5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam
CAS No.:284045-95-0
Molecular Formula:C10H17NO7
Molecular Weight:263.24
Hs Code.:
Mol file:284045-95-0.mol

Synonyms:5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam;2-Piperidinone, 3-hydroxy-4-(β-D-xylopyranosyloxy)-, (3S,4R)-

Suppliers and Price of 5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam
10mg
$ 13750.00

American Custom Chemicals Corporation
5-AMINO-3-O(BETA-D-XYLOPYRANOSYL)-D-THREOPENTANO-1,5-LACTAM 95.00%
5MG
$ 499.88

Total 7 raw suppliers

Chemical Property of 5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam

Chemical Property:

PSA：131.97000
LogP:-3.03270

Purity/Quality:

99% ^*data from raw suppliers

5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses A xylobiose-derived lactam

Technology Process of 5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam

There total 4 articles about 5-Amino-3-O(-D-xylopyranosyl)-D-threo-pentano-1,5-lactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 284045-99-4
Benzoic acid (3S,4R)-2-oxo-4-((2S,3R,4S,5R)-3,4,5-triacetoxy-tetrahydro-pyran-2-yloxy)-piperidin-3-yl ester

: 284045-95-0
(3S,4R)-3-Hydroxy-4-((2S,3R,4S,5R)-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-piperidin-2-one

Guidance literature:: With methanol; sodium methylate;
DOI:10.1021/ja0002870

Reference yield:

: 128376-91-0,869848-87-3
2,3,4-tri-O-acetyl-α-D-xylopyranosyl trichloroacetimidate

: 284045-95-0
(3S,4R)-3-Hydroxy-4-((2S,3R,4S,5R)-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-piperidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / BF₃*Et₂O / 1,2-dichloro-ethane / 2 h / 20 °C

2: 76 percent / NaOMe; MeOH

With methanol; boron trifluoride diethyl etherate; sodium methylate; In 1,2-dichloro-ethane; 1: glycosylation / 2: deacylation;
DOI:10.1021/ja0002870

Reference yield:

: 266688-40-8
5-amino-4,5-dideoxy-D-threo-pentono-1,5-lactam

: 284045-95-0
(3S,4R)-3-Hydroxy-4-((2S,3R,4S,5R)-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-piperidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / pyridine / -40 - 20 °C

2: 71 percent / BF₃*Et₂O / 1,2-dichloro-ethane / 2 h / 20 °C

3: 76 percent / NaOMe; MeOH

With pyridine; methanol; boron trifluoride diethyl etherate; sodium methylate; In 1,2-dichloro-ethane; 1: benzoylation / 2: glycosylation / 3: deacylation;
DOI:10.1021/ja0002870