Methanamine, N,N-dimethyl-1,1-bis(phenylmethoxy)-

Base Information

• Chemical Name: Methanamine, N,N-dimethyl-1,1-bis(phenylmethoxy)-
• CAS No.: 2016-04-8
• Molecular Formula: C17H21NO2
• Molecular Weight: 271.359
• Hs Code.: 2922199090
• European Community (EC) Number: 217-946-7
• DSSTox Substance ID: DTXSID20173987
• Nikkaji Number: J199.822F
• Wikidata: Q83044035
• Mol file: 2016-04-8.mol

Synonyms:N,N-Dimethylformamide dibenzyl acetal;2016-04-8;Methanamine, N,N-dimethyl-1,1-bis(phenylmethoxy)-;N,N-Dimethylformamide dibenzylacetal;1,1-bis(benzyloxy)-N,N-dimethylmethanamine;N,N-dimethyl-1,1-bis(phenylmethoxy)methanamine;1,1-Bis(benzyloxy)trimethylamine;SCHEMBL133145;dimethyl formamide dibenzylacetal;Bis(benzyloxy)methyldimethylamine;dimethyl formamide dibenzyl acetal;DTXSID20173987;EINECS 217-946-7;MFCD00014869;AKOS024348888;SB81314;Bis(benzyloxy)-N,N-dimethylmethanamine #;N,N-Dimethylformamide dibenzyl acetal, tech. 80%

Chemical Property of Methanamine, N,N-dimethyl-1,1-bis(phenylmethoxy)-

Chemical Property:

• Vapor Pressure: 3.39E-05mmHg at 25°C
• Refractive Index: n20/D 1.536(lit.)
• Boiling Point: 354.3 °C at 760 mmHg
• PKA: 5.07±0.50(Predicted)
• Flash Point: 137.1 °C
• PSA: 21.70000
• Density: 1.073 g/cm³
• LogP: 3.26520
• Sensitive.: Moisture Sensitive
• Solubility.: Soluble in variety of inert solvents.
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 7
• Exact Mass: 271.157228913
• Heavy Atom Count: 20
• Complexity: 223

Purity/Quality:

98%min ^*data from raw suppliers

N,N-Dimethylformamide dibenzyl acetal ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CN(C)C(OCC1=CC=CC=C1)OCC2=CC=CC=C2

Technology Process of Methanamine, N,N-dimethyl-1,1-bis(phenylmethoxy)-

There total 2 articles about Methanamine, N,N-dimethyl-1,1-bis(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-formamide dimethyl acetal (4637-24-5) + benzyl alcohol (100-51-6,185532-71-2) → N,N-dimethylformamide dibenzyl acetal (2016-04-8)

Guidance literature:

at 140 - 150 ℃;

DOI:10.1002/hlca.19650480734

Reference yield:

→ N,N-dimethylformamide dibenzyl acetal (2016-04-8)

Guidance literature:

entspr. Alkoholat, Cl-Verb.;

Reference yield: 99.0%

N,N-dimethylformamide dibenzyl acetal (2016-04-8) → DBC (3459-92-5)

Guidance literature:

With carbon dioxide; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 100 ℃; for 12h; under 7500.75 Torr; Temperature; Reagent/catalyst; Solvent; Autoclave;

upstream raw materials:

N,N-dimethyl-formamide dimethyl acetal

benzyl alcohol

Downstream raw materials:

benzyl 2,4,6-trimethylbenzoate

11-{[2-(2-{[(10-Benzyloxycarbonyl-decyl)-methyl-carbamoyl]-methoxy}-ethoxy)-acetyl]-methyl-amino}-undecanoic acid benzyl ester

2-(2-tert-butoxycarbonylamino-acetylamino)-3-phenyl-propionic acid benzyl ester

N--Phe-benzylester

Refernces