Methoxetamine

Base Information

• Chemical Name: Methoxetamine
• CAS No.: 1239943-76-0
• Molecular Formula: C15H21NO2
• Molecular Weight: 247.33
• Mol file: 1239943-76-0.mol

Synonyms:2-(3-Methoxyphenyl)-2-(N-ethylamino)cyclohexanone;2-(Ethylamino)-2-(3-methoxyphenyl)-1-cyclohexanone;2-(Ethylamino)-2-(3-methoxyphenyl)cyclohexanone;TX-010394;2-(Ethylamino)-2-(3-methoxyphenyl)cyclohexan-1-one;

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Chemical Property of Methoxetamine

Chemical Property:

• Boiling Point: 389.084 °C at 760 mmHg
• Flash Point: 189.111 °C
• Density: 1.076 g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methoxetamine

There total 13 articles about Methoxetamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxybenzonitrile (1527-89-5) → (±)-2-(3-methoxyphenyl)-2-(ethylamino)cyclohexanone (1239943-76-0)

Guidance literature:

Multi-step reaction with 4 steps

1: magnesium / tetrahydrofuran

2: bromine / tetrachloromethane

3: 0 °C

4: decalin / 190 °C / Microwave irradiation

With bromine; magnesium; In tetrahydrofuran; tetrachloromethane; decalin;

DOI:10.1039/c7ra10893a

Reference yield:

(m-methoxyphenyl)cyclopentyl ketone (339549-67-6) → (±)-2-(3-methoxyphenyl)-2-(ethylamino)cyclohexanone (1239943-76-0)

Guidance literature:

Multi-step reaction with 3 steps

1: bromine / tetrachloromethane

2: 0 °C

3: decalin / 190 °C / Microwave irradiation

With bromine; In tetrachloromethane; decalin;

DOI:10.1039/c7ra10893a

Reference yield:

1-((Ethylimino)(3-methoxyphenyl) methyl)cyclopentan-1-ol → (±)-2-(3-methoxyphenyl)-2-(ethylamino)cyclohexanone (1239943-76-0)

Guidance literature:

In decalin; at 190 ℃; Microwave irradiation;

DOI:10.1039/c7ra10893a

upstream raw materials:

3-methoxybenzonitrile

(m-methoxyphenyl)cyclopentyl ketone

Downstream raw materials:

(R)-(-)-methoxetamine hydrochloride

(S)-(+)-methoxetamine hydrochloride