3-AMino-4-(2-chlorophenyl)-6-nitro-2(1H)-quinolinone

Base Information

• Chemical Name: 3-AMino-4-(2-chlorophenyl)-6-nitro-2(1H)-quinolinone
• CAS No.: 55198-89-5
• Molecular Formula: C15H10ClN3O3
• Molecular Weight: 315.71
• Hs Code.: 2933499090
• Mol file: 55198-89-5.mol

Synonyms:3-amino-4-(2-chlorophenyl)-6-nitro-1H-quinolin-2-one;

Chemical Property of 3-AMino-4-(2-chlorophenyl)-6-nitro-2(1H)-quinolinone

Chemical Property:

• Boiling Point: 566.8±50.0 °C(Predicted)
• PKA: 9.18±0.70(Predicted)
• PSA: 104.96000
• Density: 1.477±0.06 g/cm3(Predicted)
• LogP: 4.85560
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature
• Solubility.: DMSO (Slightly), Methanol (Slightly, Heated, Sonicated)

Purity/Quality:

97% ^*data from raw suppliers

3-Amino-4-(2-chlorophenyl)-6-nitro-2(1H)-quinolinone(ClonazepamImpurity) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Clonazepam (C587080) impurity in active substance and tablets. Labelled Clonazepam (C587080) impurity. 3-Amino-4-(2-chlorophenyl)-6-nitro-2(1H)-quinolinone (Clonazepam EP Impurity B) is an impurity of Clonazepam (C587080), antiepileptic agent with anxiolytic and antimanic properties.

Technology Process of 3-AMino-4-(2-chlorophenyl)-6-nitro-2(1H)-quinolinone

There total 3 articles about 3-AMino-4-(2-chlorophenyl)-6-nitro-2(1H)-quinolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

2-aminoacetamido-2'-chloro-5-nitrobenzophenone (17714-02-2) → 3-Amino-4-(2-chlorphenyl)-6-nitro-2(1H)-chinolinon (55198-89-5)

Guidance literature:

With acetic acid; In acetone; for 4h; Heating;

Reference yield:

N-[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-2-{[1-phenyl-meth-(E)-ylidene]-amino}-acetamide (80837-71-4) → 3-Amino-4-(2-chlorphenyl)-6-nitro-2(1H)-chinolinon (55198-89-5)

Guidance literature:

With acetic acid; In methanol; Heating;

Reference yield:

9b-(2-Chlorphenyl)-2,2-dimethyl-8-nitro-2,3,3a,9b-tetrahydro-5H-oxazolo<4,5-c>chinolin-4-on (80837-70-3) → 3-Amino-4-(2-chlorphenyl)-6-nitro-2(1H)-chinolinon (55198-89-5)

Guidance literature:

With acetic acid; In methanol; Heating;

upstream raw materials:

N-[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-2-{[1-phenyl-meth-(E)-ylidene]-amino}-acetamide

9b-(2-Chlorphenyl)-2,2-dimethyl-8-nitro-2,3,3a,9b-tetrahydro-5H-oxazolo<4,5-c>chinolin-4-on

2-aminoacetamido-2'-chloro-5-nitrobenzophenone

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