1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide

Base Information

• Chemical Name: 1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide
• CAS No.: 608140-12-1
• Molecular Formula: C11H20F6N2O4S2
• Molecular Weight: 422.413
• European Community (EC) Number: 801-453-4
• UNII: 7EY5Y2UR2B
• ChEMBL ID: CHEMBL3188491
• DSSTox Substance ID: DTXSID4049329
• Mol file: 608140-12-1.mol

Synonyms:608140-12-1;1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide;1-Methyl-1-propylpiperidin-1-ium bis((trifluoromethyl)sulfonyl)amide;N-methyl-N-propylpiperidinium bis(trifluoromethanesulfonyl)imide;DTXSID4049329;1-Methyl-1-propylpiperidinium bis(trifluoromethanesulfonyl)imide;bis(trifluoromethylsulfonyl)azanide;1-methyl-1-propylpiperidin-1-ium;PP13TFSI;7EY5Y2UR2B;SCHEMBL924949;CHEMBL3188491;DTXCID3029285;IEFUHGXOQSVRDQ-UHFFFAOYSA-N;Tox21_202667;MFCD08458916;NCGC00260215-01;BS-49721;CAS-608140-12-1;F20705;1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)amide;N-propyl-N-methylpiperidinium bis(trifluoromethanesulfonyl)imide;1-Methyl-1-propylpiperidin-1-iumbis((trifluoromethyl)sulfonyl)amide;1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide, >=99%, H2O <=500 ppm;Piperidinium, 1-methyl-1-propyl-, salt with 1,1,1-trifluoro-N-[(trifluoromethyl)sulfonyl]methanesulfonamide (1:1)

Chemical Property of 1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide

Chemical Property:

• Melting Point: 8.7 °C(Solv: dichloromethane (75-09-2); water (7732-18-5))
• PSA: 85.04000
• Density: 1.407 g/cm3(Temp: 30 °C)
• LogP: 5.20660
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 11
• Rotatable Bond Count: 4
• Exact Mass: 422.07686844
• Heavy Atom Count: 25
• Complexity: 467

Purity/Quality:

99% ^*data from raw suppliers

1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide ≥99%, H2O ≤500?ppm ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC[N+]1(CCCCC1)C.C(F)(F)(F)S(=O)(=O)[N-]S(=O)(=O)C(F)(F)F

Technology Process of 1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide

There total 4 articles about 1-Methyl-1-propylpiperidinium bis(trifluoromethylsulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-metnhyl-N-propylpiperidinium bromide (88840-42-0) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → N-methyl-N-propylpiperidinium bis(trifluoromethanesulfonyl)imide (608140-12-1)

Guidance literature:

In water; for 1h;

Reference yield:

[1-propyl-1-methylpiperidinium]Cl (1383436-85-8) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → N-methyl-N-propylpiperidinium bis(trifluoromethanesulfonyl)imide (608140-12-1)

Guidance literature:

In dichloromethane; water; at 20 ℃; for 24h;

Reference yield:

1-propyl-1-methylpiperidinium iodide (17874-63-4) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → N-methyl-N-propylpiperidinium bis(trifluoromethanesulfonyl)imide (608140-12-1)

Guidance literature:

In water;

DOI:10.1002/chem.200902753

upstream raw materials:

1-propyl-1-methylpiperidinium iodide

bis(trifluoromethane)sulfonimide lithium

N-metnhyl-N-propylpiperidinium bromide

[1-propyl-1-methylpiperidinium]Cl

Refernces

• 1、 Xiang,Yin,Wang,Lin,Ge,Xie,Chen. "Improving electrochemical properties of room temperature ionic liquid (RTIL) based electrolyte for Li-ion batteries". . p. 5204 - 5209. Retrieved 2010.
• 2、 -. "Piperidine type ionic liquid and preparation method and application thereof". Paragraph 0036; 0043; 0049; 0053; 0057; 0061; 0071. . Retrieved 2019/05/04.