N,N'-Bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic DiiMide

Base Information

• Chemical Name: N,N'-Bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic DiiMide
• CAS No.: 82953-57-9
• Molecular Formula: C₄₈H₄₂N₂O₄
• Molecular Weight: 710.872
• Hs Code.: 29252900
• Mol file: 82953-57-9.mol

Synonyms:Anthra[2,1,9-def6,5,10-def]diisoquino-line-1,3,8,10(2H,9H)tetrone,2,9-bis[2,6-bis(1-methylethyl)phenyl]

Chemical Property of N,N'-Bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic DiiMide

Chemical Property:

• Melting Point: 295-297 °C
• PKA: 3.98±0.20(Predicted)
• PSA: 78.14000
• Density: 1.290±0.06 g/cm3(Predicted)
• LogP: 10.43500
• Solubility.: slightly sol. in Dimethylformamide

Purity/Quality:

98%,99%, ^*data from raw suppliers

N,N'-Bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic Diimide >98.0%(N) ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-Bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic DiiMide

There total 4 articles about N,N'-Bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic DiiMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

→ Lumogen F Orange 240 (82953-57-9)

Guidance literature:

With pyridine; manganese; sodium formate; cobalt(II) bromide; In N,N-dimethyl acetamide; at 100 ℃; for 8h; Temperature; Inert atmosphere; Schlenk technique;

Reference yield:

N,N'-bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic diimide anion radical → Lumogen F Orange 240 (82953-57-9) + N,N'-bis(2,6-diisopropylphenyl)-3,4,9,10-perylenetetracarboxylic diimide dianion

Guidance literature:

With tert-butylammonium hexafluorophosphate(V); In chloroform; acetonitrile; Equilibrium constant; cyclovoltammetry;

DOI:10.1021/ja984188m

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → Lumogen F Orange 240 (82953-57-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-imidazole / 24 h / 130 °C / Inert atmosphere

2: 1H-imidazole / 24 h / 130 °C

With 1H-imidazole;

upstream raw materials:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

2,6-diisopropylbenzenamine