Bis(3,5-dichloro-2,4,6-trinitrophenyl)-diazene

Base Information

• Chemical Name: Bis(3,5-dichloro-2,4,6-trinitrophenyl)-diazene
• CAS No.: 116763-58-7
• Molecular Formula: C12Cl4N8O12
• Molecular Weight: 589.9868
• Mol file: 116763-58-7.mol

Synonyms:Bis(3,5-dichloro-2,4,6-trinitrophenyl)-diazene

Chemical Property of Bis(3,5-dichloro-2,4,6-trinitrophenyl)-diazene

Chemical Property:

• Vapor Pressure: 6.93E-25mmHg at 25°C
• Boiling Point: 804.2°C at 760 mmHg
• Flash Point: 440.2°C
• PSA: 0.00000
• Density: 2.38g/cm³
• LogP: 0.00000

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bis(3,5-dichloro-2,4,6-trinitrophenyl)-diazene

There total 4 articles about Bis(3,5-dichloro-2,4,6-trinitrophenyl)-diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-3,5-dichlorobenzoic acid (56961-25-2) → 3,3',5,5'-tetrachloro-2,2',4,4',6,6'-hexanitroazobenzene (116763-58-7)

Guidance literature:

With sodium nitrate; sulfuric acid; at 93 ℃; for 5h; Temperature; Cooling with ice;

Reference yield:

3,5-Dichloroaniline (626-43-7) → 3,3',5,5'-tetrachloro-2,2',4,4',6,6'-hexanitroazobenzene (116763-58-7)

Guidance literature:

With sulfuric acid; nitric acid; at 20 - 65 ℃; for 2h; Temperature; Cooling with ice;

Reference yield:

2,6-dichloro-1-nitrobenzoic acid (69708-32-3) → 3,3',5,5'-tetrachloro-2,2',4,4',6,6'-hexanitroazobenzene (116763-58-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid; sodium azide / chloroform / 5 h / 45 °C / Cooling with ice

2: sulfuric acid; sodium nitrate / 5 h / 93 °C / Cooling with ice

With sodium nitrate; sodium azide; sulfuric acid; In chloroform;

upstream raw materials:

2,6-dichloro-1-nitrobenzoic acid

4-amino-3,5-dichlorobenzoic acid

3,5-dichlorobenzoic acid

3,5-Dichloroaniline