6-O-Trityl-1,2,3,4-tetra-O-benzoyl-α-D-mannopyranose

Base Information

• Chemical Name: 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-α-D-mannopyranose
• CAS No.: 377074-45-8
• Molecular Formula: C₅₃H₄₂O₁₀
• Molecular Weight: 838.91
• Mol file: 377074-45-8.mol

Synonyms:6-O-Trityl-1,2,3,4-tetra-O-benzoyl-α-D-mannopyranose;1,2,3,4-Tetra-O-benzoyl-6-O-trityl-a-D-mannopyranose

Chemical Property of 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-α-D-mannopyranose

Chemical Property:

• PSA: 123.66000
• LogP: 9.25380

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-α-D-mannopyranose

There total 1 articles about 6-O-Trityl-1,2,3,4-tetra-O-benzoyl-α-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trityl chloride (76-83-5) → 1,2,3,4-tetra-O-benzoyl-6-O-trityl-D-mannopyranose (377074-45-8)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 32 h / 50 °C

2: 24 h / 0 - 40 °C

With pyridine;

DOI:10.1016/S0008-6215(01)00059-3

Reference yield:

acetic anhydride (108-24-7) + 1,2,3,4-tetra-O-benzoyl-6-O-trityl-D-mannopyranose (377074-45-8) → 1,6-di-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranoside (346441-47-2)

Guidance literature:

With sulfuric acid; In dichloromethane; acetic acid; at 20 ℃; for 20h;

DOI:10.1016/S0008-6215(01)00059-3

upstream raw materials:

trityl chloride

Downstream raw materials:

1,6-di-O-acetyl-2,3,4-tri-O-benzoyl-α-D-mannopyranoside