(2,5-dimethoxybenzyl)(triphenyl)phosphonium chloride

Base Information

Chemical Name:(2,5-dimethoxybenzyl)(triphenyl)phosphonium chloride
CAS No.:174655-16-4
Molecular Formula:C₂₇H₂₆O₂P*Cl
Molecular Weight:448.929
Hs Code.:

Synonyms:(2,5-Dimethoxybenzyl)(triphenyl)phosphonium chloride; Phosphonium, [(2,5-dimethoxyphenyl)methyl]triphenyl-, chloride (1:1)

Suppliers and Price of (2,5-dimethoxybenzyl)(triphenyl)phosphonium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2,5-dimethoxybenzyl)(triphenyl)phosphonium chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2,5-dimethoxybenzyl)(triphenyl)phosphonium chloride

There total 3 articles about (2,5-dimethoxybenzyl)(triphenyl)phosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3840-27-5
2,5-dimethoxybenzyl chloride

: 603-35-0
triphenylphosphine

: 174655-16-4
(2,5-dimethoxybenzyl)triphenylphosphonium chloride

Guidance literature:: In xylene; for 22h; Heating;
DOI:10.1021/jm980572i

Reference yield:

: 33524-31-1
2,5-dimethoxybenzyl alcohol

: 174655-16-4
(2,5-dimethoxybenzyl)triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / toluene / 0.08 h / Ambient temperature

2: 87 percent / xylene / 22 h / Heating

With thionyl chloride; In toluene; xylene;
DOI:10.1021/jm980572i

Reference yield:

: 93-02-7
2,5-dimethoxybenzaldehyde

: 174655-16-4
(2,5-dimethoxybenzyl)triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol / Ambient temperature

2: SOCl₂ / toluene / 0.08 h / Ambient temperature

3: 87 percent / xylene / 22 h / Heating

With sodium tetrahydroborate; thionyl chloride; In methanol; toluene; xylene;
DOI:10.1021/jm980572i