Acetic acid14-[7a-methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-7,12-dioxo-1,2,3,4,5,7,12,14-octahydro-phthalazino[2,3-b]phthalazin-2-yl ester

Base Information

• Chemical Name: Acetic acid14-[7a-methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-7,12-dioxo-1,2,3,4,5,7,12,14-octahydro-phthalazino[2,3-b]phthalazin-2-yl ester
• CAS No.: 169737-23-9
• Molecular Formula: C38H50N2O4
• Molecular Weight: 598.8146
• Mol file: 169737-23-9.mol

Synonyms:Acetic acid14-[7a-methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-7,12-dioxo-1,2,3,4,5,7,12,14-octahydro-phthalazino[2,3-b]phthalazin-2-yl ester;Phthalazino[2,3-b]phthalazine-5,14-dione, 9-(acetyloxy)-7,8,9,10,11,12-hexahydro-7-[[octahydro-7a-methyl-1-(1,2,4-trimethyl-2-hexenyl)-4H-inden-4-ylidene]methyl]-, [1R-[1α(1R*,2E,4R*),3aβ,4E(7R*,9R*),7aα]]- (9CI)

Chemical Property of Acetic acid14-[7a-methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-7,12-dioxo-1,2,3,4,5,7,12,14-octahydro-phthalazino[2,3-b]phthalazin-2-yl ester

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 678.841°C at 760 mmHg
• Flash Point: 364.35°C
• PSA: 70.30000
• Density: 1.178g/cm³
• LogP: 7.75730

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetic acid14-[7a-methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-7,12-dioxo-1,2,3,4,5,7,12,14-octahydro-phthalazino[2,3-b]phthalazin-2-yl ester

There total 2 articles about Acetic acid14-[7a-methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-7,12-dioxo-1,2,3,4,5,7,12,14-octahydro-phthalazino[2,3-b]phthalazin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

2,3-dihydrophthalazine-1,4-dione (1445-69-8) + ergocalciferol acetate (2579-08-0) → 6(R),19-(N,N'-phthalhydrazido)-3β-acetoxy-9,10-secoergosta-5(10),7(E),22(E)-triene (87480-21-5,169737-23-9) + 6(S),19-(N,N'-phthalhydrazido)-3β-acetoxy-9,10-secoergosta-5(10),7(E),22(E)-triene (87417-00-3,169737-23-9)

Guidance literature:

With lead(IV) acetate; acetic acid; In dichloromethane; at 0 ℃;

DOI:10.1021/jo00375a013

Reference yield: 54.0%

2,3-dihydrophthalazine-1,4-dione (1445-69-8) + ergocalciferol acetate (2579-08-0) → 6(R),19-(N,N'-phthalhydrazido)-3β-acetoxy-9,10-secoergosta-5(10),7(E),22(E)-triene (87480-21-5,169737-23-9) + 6(S),19-(N,N'-phthalhydrazido)-3β-acetoxy-9,10-secoergosta-5(10),7(E),22(E)-triene (87417-00-3,169737-23-9)

Guidance literature:

With lead(IV) acetate; acetic acid; In dichloromethane; at 0 ℃;

DOI:10.1021/jo00375a013

upstream raw materials:

2,3-dihydrophthalazine-1,4-dione

ergocalciferol acetate

Refernces