BOC-L-CYCLOPROPYLALANINE-DCHA

Base Information

• Chemical Name: BOC-L-CYCLOPROPYLALANINE-DCHA
• CAS No.: 89483-06-7
• Molecular Formula: C23H42N2O4
• Molecular Weight: 229.276
• Mol file: 89483-06-7.mol

Synonyms:BOC-ALA(CPRO)-OH DCHA;BOC-ALA(CYCLOPROPYL)-OH DCHA;Boc-b-cyclopropyl-L-Ala-OH·DCHA;BOC-BETA-CYCLOPROPYL-ALA-OH DCHA;BOC-BETA-CYCLOPROPYL-ALANINE DCHA;BOC-BETA-CYCLOPROPYL-L-ALA-OH DCHA;BOC-BETA-CYCLOPROPYL-L-ALANINE DCHA;BOC-ALA(BETA-CYCLOPROPYL)-OH DICYCLOHEXYLAMMONIUM SALT;N-ALPHA-T-BUTOXYCARBONYL-3-CYCLOPROPYL-L-ALANINE DICYCLOHEXYLAMMONIUM SALT;N-ALPHA-T-BUTOXYCARBONYL-BETA-CYCLOPROPYL-L-ALANINE DICYCLOHEXYLAMMONIUM SALT;

Chemical Property of BOC-L-CYCLOPROPYLALANINE-DCHA

Chemical Property:

• Boiling Point: 377.2±25.0 °C(Predicted)
• PKA: 4.00±0.10(Predicted)
• PSA: 91.15000
• Density: 1.162±0.06 g/cm3(Predicted)
• LogP: 5.60110
• Storage Temp.: -15°C

Purity/Quality:

99% ^*data from raw suppliers

BOC-L-Cyclopropylalanine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BOC-L-CYCLOPROPYLALANINE-DCHA

There total 3 articles about BOC-L-CYCLOPROPYLALANINE-DCHA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

di-tert-butyl dicarbonate (24424-99-5) + (2S)-2-amino-3-cyclopropylpropanoic acid (102735-53-5,15785-52-1) → (2S)-2-[[(tert-butoxy)carbonyl]amino]-3-cyclopropylpropanoic acid (89483-06-7,89483-08-9)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; water;

Reference yield: 85.0%

methyl (S)-2-((tert-butoxycarbonyl)amino)-3-cyclopropylpropanoate (104347-84-4) → (2S)-2-[[(tert-butoxy)carbonyl]amino]-3-cyclopropylpropanoic acid (89483-06-7,89483-08-9)

Guidance literature:

With lithium hydroxide monohydrate; In tetrahydrofuran; water; ethyl acetate;

Reference yield: 80.0%

C11H19NO4*C6H13N → (2S)-2-[[(tert-butoxy)carbonyl]amino]-3-cyclopropylpropanoic acid (89483-06-7,89483-08-9)

Guidance literature:

With potassium hydrogensulfate; In dichloromethane; water; Cooling with ice;

DOI:10.1016/j.ejmech.2021.113194

upstream raw materials:

methyl (S)-2-((tert-butoxycarbonyl)amino)-3-cyclopropylpropanoate

di-tert-butyl dicarbonate

(2S)-2-amino-3-cyclopropylpropanoic acid

Downstream raw materials:

methyl (S)-2-((tert-butoxycarbonyl)amino)-3-cyclopropylpropanoate

(4S,5S)-5-{3-[(S)-2-({[((S)-tert-Butoxycarbonyl-phenyl-methyl)-carbamoyl]-methyl}-carbamoyl)-1-cyclopropylmethyl-2-hydroxy-ethyl]-1-cyclopropylmethyl-ureidomethyl}-4-cyclohexyl-2,2-dimethyl-oxazolidine-3-carboxylic acid isobutyl ester

(S)-[2-((S)-3-{(S)-2-[((S)-2-Cyclohexyl-2-isobutoxycarbonylamino-acetyl)-methyl-amino]-3-cyclopropyl-propionylamino}-4-cyclopropyl-2-hydroxy-butyrylamino)-acetylamino]-phenyl-acetic acid tert-butyl ester

(4S,5S)-5-{3-[2-({[((S)-tert-Butoxycarbonyl-phenyl-methyl)-carbamoyl]-methyl}-carbamoyl)-1-cyclopropylmethyl-2-oxo-ethyl]-1-cyclopropylmethyl-ureidomethyl}-4-cyclohexyl-2,2-dimethyl-oxazolidine-3-carboxylic acid isobutyl ester

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