THIODIACETONE

Base Information

• Chemical Name: THIODIACETONE
• CAS No.: 63578-76-7
• Molecular Formula: C6H10O2S
• Molecular Weight: 146.21
• Mol file: 63578-76-7.mol

Synonyms:

Chemical Property of THIODIACETONE

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of THIODIACETONE

There total 2 articles about THIODIACETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroacetone (78-95-5) → 4-thiaheptane-2,6-dione (63578-76-7) + 1-mercaptopropan-2-one (24653-75-6)

Guidance literature:

With sodium hydrogensulfide; water; at 0 ℃;

Reference yield:

water (7732-18-5) + chloroacetone (78-95-5) → 4-thiaheptane-2,6-dione (63578-76-7) + 1-mercaptopropan-2-one (24653-75-6)

Guidance literature:

at 0 ℃;

Reference yield: 24.0%

4-thiaheptane-2,6-dione (63578-76-7) + 4-Ethoxyaniline (156-43-4) → C14H21NOS

Guidance literature:

With 5A molecular sieve; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; toluene-4-sulfonic acid; In toluene; at 50 ℃; for 48h;

DOI:10.1055/s-2007-984877

upstream raw materials:

chloroacetone

water

Downstream raw materials:

4-thia-heptane-2,6-dione-bis-(2,4-dinitro-phenylhydrazone)