2,4-Difluoro-6-iodoaniline

Base Information

• Chemical Name: 2,4-Difluoro-6-iodoaniline
• CAS No.: 582319-15-1
• Molecular Formula: C6H4F2IN
• Molecular Weight: 255.006
• Hs Code.: 2921420090

Synonyms:2-Amino-3,5-difluoroiodobenzene; 2,4-Difluoro-6-iodobenzenamine

Chemical Property of 2,4-Difluoro-6-iodoaniline

Chemical Property:

• Boiling Point: 231℃
• PKA: 1.20±0.10(Predicted)
• Flash Point: 93℃
• PSA: 26.02000
• Density: 2.086
• LogP: 2.73280
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

98%Min ^*data from raw suppliers

2,4-Difluoro-6-iodoaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-Difluoro-6-iodoaniline

There total 1 articles about 2,4-Difluoro-6-iodoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,4-difluorophenylamine (367-25-9,76563-56-9) → 2,4-difluoro-6-iodo-aniline (582319-15-1)

Guidance literature:

With iodine; iodic acid; In 1,4-dioxane; water; for 3h; Reflux;

DOI:10.1016/j.jfluchem.2011.09.008

Reference yield: 89.0%

2,4-difluoro-6-iodo-aniline (582319-15-1) + trimethylsilylacetylene (1066-54-2) → 2,4-difluoro-6-[(trimethylsilyl)ethynyl]aniline (684250-21-3)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 40 ℃; Inert atmosphere;

Reference yield: 77.0%

2,4-difluoro-6-iodo-aniline (582319-15-1) + phenylacetylene (536-74-3) → C14H9F2N (1363411-84-0)

Guidance literature:

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; sodium acetate; triethylamine; at 70 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.jfluchem.2011.09.008

upstream raw materials:

2,4-difluorophenylamine

Downstream raw materials:

2-ethynyl-4,6-difluoroaniline

C₁₄H₁₅F₂NO₂

C₁₄H₉F₂N

C₁₂H₁₃F₂N

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