Saxagliptin interMediate B

Base Information

Chemical Name:Saxagliptin interMediate B
CAS No.:1110783-95-3
Molecular Formula:C₁₇H₂₇NO₅
Molecular Weight:329.383
Hs Code.:

Synonyms:SAXAGLIPTIN INTERMEDIATE B;(alphaS)-alpha-[[(1,1-dimethylethoxy)carbonyl]amino]-3-hydroxy-Tricyclo[3.3.1.1(3,7)]decane-1-acetic-carboxy-14C acid

Suppliers and Price of Saxagliptin interMediate B

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 21 raw suppliers

Chemical Property of Saxagliptin interMediate B

Chemical Property:

Purity/Quality:: 98%Min ^*data from raw suppliers

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Technology Process of Saxagliptin interMediate B

There total 2 articles about Saxagliptin interMediate B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [1,2-14C]-2-oxo-2-(3'-hydroxyadamant-1'-yl)acetic acid

: 24424-99-5
di-tert-butyl dicarbonate

: 1110783-95-3
(S)-N-Boc-[1,2-14C]-2-(3'-hydroxyadamant-1'-yl)glycine

Guidance literature:: [1,2-14C]-2-oxo-2-(3'-hydroxyadamant-1'-yl)acetic acid; With sodium hydroxide; ammonium formate; nicotinamide adenine dinucleotide; diothiothreitol; In water; at 40 ℃; for 100h; pH=8.0;

di-tert-butyl dicarbonate; In tetrahydrofuran; water; at 20 ℃; for 3h; pH=13; Further stages.;
DOI:10.1002/jlcr.1450