1-Chloro-1-methylsilacyclopentane

Base Information

• Chemical Name: 1-Chloro-1-methylsilacyclopentane
• CAS No.: 2406-31-7
• Molecular Formula: C5H11ClSi
• Molecular Weight: 134.681
• Mol file: 2406-31-7.mol

Synonyms:1-chloro-1-methyl-1-silacyclopentane;1-Chlor-1-methyl-silolan;1-Chlor-1-methyl-silacyclopentan;1-chloro-1-methyl-silolane;

Chemical Property of 1-Chloro-1-methylsilacyclopentane

Chemical Property:

• Boiling Point: 128℃
• Flash Point: 22℃
• PSA: 0.00000
• Density: 0.96
• LogP: 2.59430

Purity/Quality:

99.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Chloro-1-methylsilacyclopentane

There total 6 articles about 1-Chloro-1-methylsilacyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

Methyltrichlorosilane (75-79-6) + 1,4-dichlorobutane (110-56-5) → methyl(tetramethylene)silyl chloride (2406-31-7)

Guidance literature:

With magnesium; ethylene dibromide; In dibutyl diglyme; at 20 - 95 ℃; for 5h;

Reference yield:

Methyltrichlorosilane (75-79-6) + 1,4-bis(bromomagnesium)butane (23708-47-6) → methyl(tetramethylene)silyl chloride (2406-31-7)

Guidance literature:

With diethyl ether;

DOI:10.1021/ja01652a036

Reference yield:

1-(3-chloro-propyl)-1-methyl-silolane (3944-23-8) → methyl(tetramethylene)silyl chloride (2406-31-7)

Guidance literature:

With aluminium trichloride;

DOI:10.1007/BF00846201

upstream raw materials:

Methyltrichlorosilane

1,4-bis(bromomagnesium)butane

1,4-dibromo-butane

1-(3-chloro-propyl)-1-methyl-silolane