2-Bromo-9,9-bis(2-ethylhexyl)fluorene

Base Information

Chemical Name:2-Bromo-9,9-bis(2-ethylhexyl)fluorene
CAS No.:355135-07-8
Molecular Formula:C29H41Br
Molecular Weight:469.54
Hs Code.:
European Community (EC) Number:807-970-1
DSSTox Substance ID:DTXSID00460029
Nikkaji Number:J2.273.467I
Mol file:355135-07-8.mol

Synonyms:2-bromo-9,9-bis(2-ethylhexyl)fluorene;355135-07-8;2-BROMO-9,9-BIS(2-ETHYLHEXYL)-9H-FLUORENE;2-Bromo-9,9-bis(2-ethylhexyl)fluoren;2-BROMO-9,9-BIS(2-ETHYL-HEXYL)-FLUOREN;SCHEMBL9898232;DTXSID00460029;JAWAIXIROBPNSH-UHFFFAOYSA-N;MFCD12024275;AKOS037645724;2-bromo-9,9-di(2-ethylhexyl)-fluorene;AS-62723;B4441;T70818

Suppliers and Price of 2-Bromo-9,9-bis(2-ethylhexyl)fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
2-Bromo-9,9-bis(2-ethylhexyl)fluorene >98.0%(GC)
1g
$ 260.00

AK Scientific
2-Bromo-9,9-bis(2-ethylhexyl)fluorene
1g
$ 398.00

Total 8 raw suppliers

Chemical Property of 2-Bromo-9,9-bis(2-ethylhexyl)fluorene

Chemical Property:

Refractive Index:1.5530-1.5570
PSA：0.00000
LogP:9.92860
XLogP3:12.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:12
Exact Mass:468.23916
Heavy Atom Count:30
Complexity:467

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-9,9-bis(2-ethylhexyl)fluorene >98.0%(GC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC(CC)CC1(C2=CC=CC=C2C3=C1C=C(C=C3)Br)CC(CC)CCCC

Technology Process of 2-Bromo-9,9-bis(2-ethylhexyl)fluorene

There total 2 articles about 2-Bromo-9,9-bis(2-ethylhexyl)fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.8%

: 18908-66-2
3-bromomethylheptane

: 1133-80-8
2-bromo-9H-fluorene

: 355135-07-8
2-bromo-9,9-bis(2-ethylhexyl)fluorene

Guidance literature:: With potassium iodide; potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.jfluchem.2015.07.027

Reference yield:

: 86-73-7
9H-fluorene

: 355135-07-8
2-bromo-9,9-bis(2-ethylhexyl)fluorene

Guidance literature:: Multi-step reaction with 2 steps

1.1: iron(III) chloride; N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h / 20 °C / Darkness

2.1: potassium iodide; potassium hydroxide / dimethyl sulfoxide / 0.5 h

2.2: 24 h / 20 °C

With iron(III) chloride; N-Bromosuccinimide; potassium iodide; potassium hydroxide; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.14233/ajchem.2014.16346