17-aza-homo-delta (1,3,5(10)) estratrien-3-ol-17-one-4-N,N-bis(2-chloroethyl)aminophenylacetate

Base Information

• Chemical Name: 17-aza-homo-delta (1,3,5(10)) estratrien-3-ol-17-one-4-N,N-bis(2-chloroethyl)aminophenylacetate
• CAS No.: 87777-66-0
• Molecular Formula: C30H36 Cl2 N2 O3
• Molecular Weight: 543.53

Synonyms:Naphtho[2,1-f]quinoline,17a-aza-D-homoestra-1,3,5(10)-trien-17-one deriv.

Chemical Property of 17-aza-homo-delta (1,3,5(10)) estratrien-3-ol-17-one-4-N,N-bis(2-chloroethyl)aminophenylacetate

Chemical Property:

• Vapor Pressure: 2.26E-21mmHg at 25°C
• Melting Point: 124 - 126 °C (diethyl ether)
• Boiling Point: 733.5°C at 760 mmHg
• Flash Point: 397.4°C
• PSA: 58.64000
• Density: 1.236g/cm³
• LogP: 6.17220

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of 17-aza-homo-delta (1,3,5(10)) estratrien-3-ol-17-one-4-N,N-bis(2-chloroethyl)aminophenylacetate

There total 1 articles about 17-aza-homo-delta (1,3,5(10)) estratrien-3-ol-17-one-4-N,N-bis(2-chloroethyl)aminophenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

8-hydroxy-12a-methyl-3,4,4a,4b,5,6,10b,11,12,12a-decahydronaphtho[2,1-f]quinolin-2(1H)-one (1616-20-2) + 4-bis(2-chloroethyl)aminophenylacetic acid (10477-72-2) → {4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-acetic acid (4aS,4bR,10bS,12aS)-12a-methyl-2-oxo-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-1-aza-chrysen-8-yl ester (87777-66-0)

Guidance literature:

With dicyclohexyl-carbodiimide; dmap; In dichloromethane; for 200h; Ambient temperature;

upstream raw materials:

8-hydroxy-12a-methyl-3,4,4a,4b,5,6,10b,11,12,12a-decahydronaphtho[2,1-f]quinolin-2(1H)-one

4-bis(2-chloroethyl)aminophenylacetic acid

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