Trifluoro-Methanesulfonicacid2-Methoxy-4-forMyl-6-nitro-phenylester

Base Information

• Chemical Name: Trifluoro-Methanesulfonicacid2-Methoxy-4-forMyl-6-nitro-phenylester
• CAS No.: 1021493-52-6
• Molecular Formula: C9H6F3NO7S
• Molecular Weight: 329.21
• Hs Code.: 2912499000
• Mol file: 1021493-52-6.mol

Synonyms:Trifluoro-Methanesulfonicacid2-Methoxy-4-forMyl-6-nitro-phenylester

Chemical Property of Trifluoro-Methanesulfonicacid2-Methoxy-4-forMyl-6-nitro-phenylester

Chemical Property:

• PSA: 123.87000
• LogP: 3.24830
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

TrifluoromethanesulfonicAcid2-Methoxy-4-formyl-6-nitro-phenylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Trifluoro-Methanesulfonicacid2-Methoxy-4-forMyl-6-nitro-phenylester

There total 2 articles about Trifluoro-Methanesulfonicacid2-Methoxy-4-forMyl-6-nitro-phenylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

isonitrovanillin (6635-20-7) → C9H6F3NO7S (1021493-52-6)

Guidance literature:

With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 0 - 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1002/chem.201003489

Reference yield: 95.0%

trifluoromethylsulfonic anhydride (358-23-6) + isonitrovanillin (6635-20-7) → C9H6F3NO7S (1021493-52-6)

Guidance literature:

In dichloromethane; at 0 ℃;

DOI:10.1055/s-2007-1000866

Reference yield: 92.0%

C9H6F3NO7S (1021493-52-6) → C9H8F3NO7S (1315455-04-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; for 1.25h; Inert atmosphere;

DOI:10.1002/chem.201003489

upstream raw materials:

trifluoromethylsulfonic anhydride

isonitrovanillin

Downstream raw materials:

4-iodo-3-methoxy-5-nitrobenzaldehyde

C₉H₈F₃NO₇S

C₁₅H₂₂F₃NO₇SSi

C₁₉H₂₉NO₈Si

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