2-Bromo-6-Isopropylpyridine

Base Information

• Chemical Name: 2-Bromo-6-Isopropylpyridine
• CAS No.: 1037223-35-0
• Molecular Formula: C8H10BrN
• Molecular Weight: 200.078
• Hs Code.: 2933399090
• Mol file: 1037223-35-0.mol

Synonyms:2-bromo-6-propan-2-ylpyridine;

Chemical Property of 2-Bromo-6-Isopropylpyridine

Chemical Property:

• PSA: 12.89000
• LogP: 2.96750
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

2-BROMO-6-ISOPROPYLPYRIDINE 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Bromo-6-Isopropylpyridine

There total 4 articles about 2-Bromo-6-Isopropylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

2,6-Dibromopyridine (626-05-1) → 2-bromo-6-(propan-2-yl)pyridine (1037223-35-0)

Guidance literature:

In tetrahydrofuran; at -78 ℃;

DOI:10.1016/j.tetlet.2008.03.096

Reference yield: 61.0%

2,6-Dibromopyridine (626-05-1) + isopropylmagnesium chloride (1068-55-9) → 2-bromo-6-(propan-2-yl)pyridine (1037223-35-0)

Guidance literature:

isopropylmagnesium chloride; With copper(l) cyanide; lithium chloride; In tetrahydrofuran; at -78 ℃; for 0.5h;

2,6-Dibromopyridine; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1002/asia.201300440

Reference yield: 39.0%

2,6-Dibromopyridine (626-05-1) + isopropyl magnesium chloride - lithium chloride complex → 2-bromo-6-(propan-2-yl)pyridine (1037223-35-0)

Guidance literature:

isopropyl magnesium chloride - lithium chloride complex; With copper(l) cyanide; lithium chloride; In tetrahydrofuran; diethyl ether; at -78 ℃; for 2.25h; Inert atmosphere;

2,6-Dibromopyridine; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/jacs.8b06398

upstream raw materials:

2,6-Dibromopyridine

isopropylmagnesium chloride

Downstream raw materials:

6-(1-methylethyl)-2-pyridinamine

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